Pharmacognosy Lab: Extraction and Separation Techniques Quiz

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Questions and Answers

What is the primary purpose of extraction techniques in pharmacognosy?

  • To create a pure form of the plant material
  • To destroy the inactive components of the plant material
  • To separate the medicinally active constituents from the inert components (correct)
  • To alter the chemical structure of the active constituents

What is the term used to describe the products obtained from plants through extraction techniques?

  • Crude drugs
  • Phytochemicals
  • Pharmaceuticals
  • Galenical (correct)

Which of the following methods of extraction involves soaking the plant material with a cold solvent?

  • Percolation
  • Infusion
  • Decoction
  • Maceration (correct)

What is the principle of the Soxhlet apparatus method of extraction?

<p>Continuous hot extraction (D)</p> Signup and view all the answers

Which of the following is NOT a hot method of extraction?

<p>Maceration (B)</p> Signup and view all the answers

What is the primary purpose of using water in the solvent mixture during maceration?

<p>To facilitate the dissolution of alkaloids present in a salt form (B)</p> Signup and view all the answers

What is the significance of occasional agitation and staring during the maceration process?

<p>To facilitate the diffusion of the solvent into the plant material (B)</p> Signup and view all the answers

Why is chloroform used as a solvent in the extraction of volatile oils and terpenes?

<p>Due to its non-polar nature, which enables the extraction of volatile oils and terpenes (D)</p> Signup and view all the answers

What is the primary difference between the maceration and percolation methods of extraction?

<p>The method of adding the solvent to the plant material (D)</p> Signup and view all the answers

Why is the maceration process often repeated several times?

<p>Due to the difficulty in obtaining the active constituent in a single maceration process (A)</p> Signup and view all the answers

What is the purpose of allowing the plant material to macerate for 24 hours during the percolation process?

<p>To enhance the extraction of the active constituents (D)</p> Signup and view all the answers

What is the primary advantage of using a Soxhlet apparatus compared to ordinary reflux?

<p>It prevents the plant material from being directly exposed to heat (D)</p> Signup and view all the answers

What is the purpose of the thimble in a Soxhlet apparatus?

<p>To separate the plant material from the solvent (A)</p> Signup and view all the answers

What is a common requirement for the Clevenger method and the reflux method?

<p>All of the above (D)</p> Signup and view all the answers

What is the role of the condenser in the Soxhlet apparatus and the Clevenger method?

<p>To cool the solvent (B)</p> Signup and view all the answers

Why is filtration not required in the Soxhlet apparatus method?

<p>Because the thimble separates the plant material from the solvent (C)</p> Signup and view all the answers

What is the main difference between the Soxhlet apparatus and the reflux method in terms of plant material placement?

<p>The plant material is placed in the thimble in the Soxhlet apparatus (D)</p> Signup and view all the answers

Which hot method involves extraction using boiled water in an infusion pot?

<p>Decoction (B)</p> Signup and view all the answers

Which of the following plant parts is NOT suitable for extraction using the decoction method?

<p>Petals (C)</p> Signup and view all the answers

In which hot extraction method is the active constituent dissolved in a heated solvent after agitation?

<p>Digestion (C)</p> Signup and view all the answers

Which method involves allowing the volatile oil to evaporate with steam during extraction?

<p>Infusion (D)</p> Signup and view all the answers

Which factor determines the choice of solvent in hot extraction methods?

<p>The active constituent being extracted (D)</p> Signup and view all the answers

In the extraction procedure involving an

<p>2- Decoction (D)</p> Signup and view all the answers

What is the purpose of using a Soxhlet apparatus?

<p>To continuously extract active compounds using boiled solvent (C)</p> Signup and view all the answers

Which method involves actively boiling the solvent with a reflux condenser?

<p>Reflux method (D)</p> Signup and view all the answers

In continuous hot extraction method A, what is the primary purpose of the round bottom flask?

<p>To hold the plant material for extraction (A)</p> Signup and view all the answers

What distinguishes the Soxhlet method from the ordinary hot extraction method?

<p>The continuous extraction process (B)</p> Signup and view all the answers

What is the key difference between the reflux method and the Soxhlet apparatus?

<p>The need for continuous boiling of the solvent (B)</p> Signup and view all the answers

Which apparatus requires the use of a porous thimble during the extraction process?

<p>Soxhlet apparatus (B)</p> Signup and view all the answers

Flashcards

Purpose of extraction in pharmacognosy

Separating medicinally active constituents from inert components in plants.

Products from plant extraction

Galenicals

Maceration extraction

Soaking plant material in a cold solvent.

Soxhlet extraction principle

Continuous hot extraction using a special apparatus.

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Non-hot extraction method

Maceration (using cold solvent).

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Water's role in maceration

Dissolving alkaloids (in salt form).

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Maceration agitation purpose

Facilitating solvent diffusion into plant material.

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Chloroform use in extraction

Extracting non-polar compounds (volatile oils, terpenes).

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Maceration vs. Percolation difference

How the solvent is added to the plant material.

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Repeating maceration purpose

Improving active constituent extraction.

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Soxhlet apparatus advantage

Plant material isn't directly exposed to heat.

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Soxhlet thimble role

Separates plant material from solvent.

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Requirement for Clevenger/reflux

All extraction methods require a condenser.

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Soxhlet filtration need

No filtration is necessary, thimble takes care of it.

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Soxhlet vs. reflux placement

Plant material in thimble (Soxhlet), directly in flask (reflux).

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Decoction method

Using boiled water in an infusion pot.

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Unsuitable decoction plant part

Petals

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Digestion extraction method

Active constituent dissolves in a heated solvent after agitation.

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Infusion method

Volatile oil evaporates with steam.

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Solvent choice in hot extraction

Determined by the specific active constituent being extracted.

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Soxhlet apparatus purpose

Continuous extraction of active compounds using a boiled solvent.

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Reflux method

Actively boiling solvent with a reflux condenser.

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Round bottom flask purpose (continuous hot)

Holds the plant material for extraction.

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Soxhlet vs. ordinary hot extraction difference

Continuous extraction process in Soxhlet.

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Reflux vs. Soxhlet apparatus difference

Soxhlet uses continuous boiling, reflux doesn't.

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Apparatus requiring a porous thimble

Soxhlet apparatus.

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Study Notes

Extraction and Separation Techniques

  • Extraction involves separating the medicinally active constituent from the inactive component of plants or animal tissues using a solvent and a standard extraction procedure.
  • The obtained products are relatively impure liquids, semisolid, or powders, intended for oral or external use, and are called Galenical.

Methods of Extraction

  • Cold methods:
    • Maceration: extracts active compounds with a cold solvent by soaking the plant material with the solvent.
    • Percolation: extracts active compounds with a cold solvent using a percolator with a porous diaphragm at the bottom.

Hot Methods

  • Infusion: extracts active compounds with boiled water using an infusion pot.
  • Decoction: extracts active compounds with a continuously heated solvent, used for hard plant parts like barks, stems, and roots.
  • Digestion: extracts active compounds with a gentle heated solvent, used where moderate temperature is required.
  • Continuous hot extraction methods:
    • Ordinary reflux condenser: extracts active compounds with a boiled solvent using a reflux condenser.
    • Soxhlet apparatus: continuously extracts active compounds with a boiled solvent using a Soxhlet apparatus.

Solvents

  • Depend on the active constituent (alkaloids, glycosides, etc.)
  • Examples: alcohol, water, chloroform, and ether.

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