Metal Analysis using OES Techniques
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Questions and Answers

What is the primary purpose of the spectro lab?

  • To manufacture wheels directly
  • To analyze the composition of metal samples (correct)
  • To create electric arc furnaces
  • To conduct research on tungsten electrodes

Which instrument is used for testing the metal samples?

  • ARL Metal Analyzer (M-402) (correct)
  • Infrared Spectrophotometer
  • Gas Chromatograph
  • Mass Spectrometer

Which element is NOT listed among the acquired element compositions?

  • Copper
  • Silicon
  • Titanium
  • Boron (correct)

What phenomenon is employed to excite the electrons in the sample?

<p>Arc discharge (B)</p> Signup and view all the answers

What is one of the main advantages of using an optical emission spectrometer?

<p>Stability and low detection limits (C)</p> Signup and view all the answers

What principle does the hydrogen testing machine operate on?

<p>Wheatstone bridge (B)</p> Signup and view all the answers

What atmosphere is used during the spark discharge process?

<p>Argon (A)</p> Signup and view all the answers

How does the intensity of the emission spectrum correlate with the sample?

<p>It depends on the concentration of the element in the sample. (A)</p> Signup and view all the answers

How does nitrogen gas contribute to the functioning of the hydrogen testing machine?

<p>It is continuously supplied for consistent resistance. (B)</p> Signup and view all the answers

What percentage of PLC does RWF use in its processes?

<p>95% (D)</p> Signup and view all the answers

What does the emission spectrum consist of?

<p>A collection of spectral lines specific to each element (A)</p> Signup and view all the answers

What was noted as a fascinating machine during the internship?

<p>Long Forging Machine (A)</p> Signup and view all the answers

What role do photo multiplier tubes play in the analysis?

<p>They measure the presence and intensity of the spectrum. (D)</p> Signup and view all the answers

Which type of electrodes is involved in the optical emission spectrometry process?

<p>Tungsten electrodes (D)</p> Signup and view all the answers

What distinguishes the Electric Arc Furnace from other furnaces?

<p>The charge is directly exposed to an electric arc. (C)</p> Signup and view all the answers

What type of testing method is described as 'magnaglo testing'?

<p>A non-destructive testing method (D)</p> Signup and view all the answers

What effect does the excitation source have on the metal sample?

<p>It vaporizes the atoms for analysis. (A)</p> Signup and view all the answers

What best describes the process used in optical emission spectrometry?

<p>Statistical processing of emission spectra from spark discharges (A)</p> Signup and view all the answers

Which of the following is a characteristic feature of the advanced processes used at RWF?

<p>CNC (Computer Numerical Control) (A)</p> Signup and view all the answers

What aspect of the internship did the participants find thought-provoking?

<p>The communication and connectivity of workflow (B)</p> Signup and view all the answers

Flashcards

Optical Emission Spectrometry

A technique used to determine the composition of metals in a sample by analyzing the light emitted from excited atoms.

ARL Metal Analyzer (M-402)

A type of instrument used in spectro labs to analyze metal samples.

Discharge Plasma

A high-energy state created by applying electrical energy to a metal sample, causing atoms to emit light.

Excitation Source

A source of energy used to excite atoms in optical emission spectrometry, often using a spark discharge.

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Emission Spectrum

The unique pattern of light emitted by an element, used to identify its presence and quantity in a sample.

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Diffraction Grating

A device that splits light into its different wavelengths, allowing the analysis of the emission spectrum.

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Detectors (Photo multiplier tubes)

Electronic devices that measure the intensity of light emitted from specific elements in a sample.

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Qualitative and Quantitative Analysis

The process of determining the presence and concentration of elements in a sample by analyzing their emission spectra.

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Intensity of Emission Spectrum

The amount of light emitted by an element is directly proportional to its concentration in the sample.

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Spectrochemical Analysis in Wheel Manufacturing

The spectrochemical analysis of metal samples plays an important role in ensuring the quality of the metal used in wheel manufacturing.

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Wheatstone Bridge

The process of measuring the resistance of an unknown resistor by balancing it against known resistors in a circuit.

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Hydrogen Testing

A measure of the amount of hydrogen present in a material, often used to determine its strength and quality.

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Programmable Logic Control (PLC)

A type of control system used to automate processes in industries like steel making. It uses programmable instructions to control machines and equipment.

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Computer Numerical Control (CNC)

A type of control system used in manufacturing to create complex parts with precise control over movement and tools.

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Electric Arc Furnace

A method of heat treatment for steel that uses a high-temperature electric arc to melt the material.

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Magnaglo Testing

A technique where a magnetic field is used to detect surface cracks and flaws in metal parts. It uses magnetic particles that clump around defects.

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Forging

The process of shaping metal by applying force, causing it to deform without breaking.

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Furnace

A type of furnace used in steelmaking that uses heat to melt and refine the metal.

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Heat Treatment

A process used for treating materials, often involving heat and/or chemical changes.

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Study Notes

Spectro Lab

  • The lab tests samples (solidified metal) obtained from an electric arc furnace to analyze metal composition.
  • ARL Metal Analyzer (M-402 optical emission spectrometer) is used for this analysis.

Optical Emission Spectrometry (OES) Principle

  • OES applies electrical energy (spark) between electrodes (tungsten) and a metal sample.
  • This vaporizes atoms, bringing them to a high energy state (discharge plasma).
  • Excited atoms/ions in the plasma create unique emission spectra specific to each element.

Working of OES

  • Sample is placed between tungsten electrodes.
  • An electric arc is created, exciting electrons.
  • ICP (inductively coupled plasma) used as excitation source.
  • Spark, direct current arc, or glow discharge used to generate excitation.
  • Statistical processing of spark discharge spectra is done in an inert (argon) atmosphere.
  • Unique emission spectra are obtained.

Spectral Analysis

  • The emitted light is split by a diffraction grating.
  • This isolates spectral lines, extracting the emission spectrum of target elements.
  • Intensity of each element's emission spectrum is linked to its concentration in the sample.
  • Detectors (photomultiplier tubes) measure the presence/absence and intensity of the spectrum.
  • Qualitative and quantitative analysis of elements is performed based on extracted data.

Elements Analyzed

  • Carbon
  • Manganese
  • Silicon
  • Phosphorous
  • Sulphur
  • Chromium
  • Nickel
  • Copper
  • Molybdenum
  • Aluminium
  • Vanadium
  • Lead
  • Titanium
  • Tin

Advantages of Optical Emission Spectrometry (OES)

  • High speed
  • High accuracy
  • High precision
  • Low detection limits
  • Easy integration and efficiency.

Hydrogen Testing Machine

  • Tests for hydrogen and other supplementary gases.
  • Based on Wheatstone bridge principle.
  • Measures unknown electrical resistance using known resistors.
  • Nitrogen gas maintained at constant rate for resistance equalization.
  • Hydrogen diffusion rate determined based on normal distribution within Anhydrone.

Conclusion - Internship

  • The internship focused on implementing theoretical concepts on a large scale.
  • Machine operation and work flow within RWF were emphasized.
  • RWF uses 95% programmable logic controllers (PLC) and advanced processes use computer numerical control (CNC).
  • Long forging machine's power drive and capacity/plastic deformation are noted.
  • Wheel shop's Electric Arc Furnace process is unique (direct arc exposure of charge).
  • Electromechanical overhead travelling cranes (EOTs) were helpful in applications and mechanical understanding.

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Related Documents

Spectro Lab PDF

Description

Explore the principles and workings of Optical Emission Spectrometry (OES) in analyzing metal compositions. This quiz covers the application of electrical energy in producing unique emission spectra and the processes involved in spectrochemical analysis. Test your knowledge of the technology and methodologies utilized in the metal testing process.

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