Chemistry: Distillation Process
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Chemistry: Distillation Process

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Questions and Answers

What is the effect of temperature on the rate of evaporation?

  • The rate of evaporation is independent of the temperature.
  • The rate of evaporation is directly proportional to the temperature. (correct)
  • The rate of evaporation decreases as the temperature increases.
  • The rate of evaporation is inversely proportional to the temperature.
  • What is the primary difference between evaporation and boiling?

  • Evaporation is a faster process, while boiling is slower.
  • Evaporation is only possible at high temperatures, while boiling can occur at low temperatures.
  • Evaporation occurs at the boiling point of a liquid, while boiling occurs below it.
  • Evaporation occurs on the surface of a liquid, while boiling occurs throughout the liquid. (correct)
  • What type of distillation involves the use of steam?

  • Vacuum distillation
  • Fractional distillation
  • Simple distillation
  • Steam distillation (correct)
  • What is the purpose of the condenser in a distillation apparatus?

    <p>To cool the vapor</p> Signup and view all the answers

    What is the difference between simple and fractional distillation?

    <p>Simple distillation is used for pure substances, while fractional distillation is used for mixtures.</p> Signup and view all the answers

    Why is it necessary to evaporate extremely heat sensitive substances under reduced pressure?

    <p>To prevent decomposition of the substances</p> Signup and view all the answers

    What is the effect of increasing the surface area of the content vessel on the rate of evaporation?

    <p>It increases the rate of evaporation</p> Signup and view all the answers

    What is the effect of atmospheric aqueous vapour pressure on the rate of evaporation?

    <p>High vapour pressure decreases the rate of evaporation</p> Signup and view all the answers

    Why is agitation necessary during evaporation?

    <p>To prevent the formation of a scum or a layer at the upper layers of the liquid</p> Signup and view all the answers

    What is the effect of atmospheric pressure on the liquid under evaporation?

    <p>The rate of evaporation is inversely proportional to the atmospheric pressure</p> Signup and view all the answers

    Study Notes

    Distillation

    • Definition: Distillation is the process of vaporizing a liquid, re-condensing it, and collecting it in a container.
    • Boiling point of mixtures depends on mole fraction of the component present.
    • In pure substances, temperature remains constant during distillation as long as both vapor and liquid are present.
    • In miscible liquid mixtures, temperature increases throughout the process because the composition of vapor changes continuously.

    Types of Distillation

    • Simple distillation
    • Fractional distillation
    • Steam distillation
    • Vacuum distillation
    • Destructive distillation

    Distillation Apparatus

    • Heat source
    • Still pot
    • Still head
    • Thermometer/Boiling point temperature
    • Condenser
    • Cooling water in and out
    • Distillate/receiving flask
    • Vacuum/gas inlet
    • Still receiver
    • Heat control
    • Stirrer speed control
    • Stirrer/heat plate
    • Heating (Oil/sand) bath
    • Stirrer bar/anti-bumping granules
    • Cooling bath

    Evaporation

    Introduction

    • Evaporation is a type of vaporization that occurs only on the surface of a liquid.
    • Theoretically, evaporation means the free escape of vapors from the surface of a liquid below its boiling point.

    Factors Affecting Evaporation

    • Temperature: rate of evaporation is directly proportional to temperature.
    • Surface area: rate of evaporation is directly proportional to the surface area of the content vessel exposed.
    • Agitation: stirring or agitating the solution prevents decomposition of the preparation at the bottom of the container.
    • Atmospheric aqueous vapour pressure: rate of evaporation is affected by atmospheric moisture content.
    • Atmospheric pressure on the liquid under evaporation: rate of evaporation is inversely proportional to atmospheric pressure on the surface of the liquid.

    Importance of Temperature in Evaporation

    • Maximum evaporation is attained at the boiling point of the liquid.
    • Thermostable preparations can be evaporated at higher temperatures, while thermolabile preparations require low temperatures.
    • Extremely heat-sensitive substances are evaporated under reduced pressure.
    • Time required for evaporation is critical, and evaporation should be carried out for a short time at low temperature.

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    Description

    Learn about the distillation process, where a liquid is vaporized and re-condensed, and how the boiling point of mixtures depends on the mole fraction of components.

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