Reflux process with T-450

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Questions and Answers

Explain how the feed stream from T-440 is introduced into T-450 (C14 Tower), detailing the purpose of each component it encounters before entering the tower.

The feed stream from T-440 first passes through F-453 (C14 Tower Feed Strainer) to remove particulate matter. It then enters T-450 between the top and bottom beds via a chimney tray, which delivers the liquid to a feed distributor tray for even distribution onto the bottom bed, ensuring proper vapor/liquid contact.

Describe the path of the overhead vapor from T-450, including the condensers it passes through and their respective cooling media.

The overhead vapor from T-450 goes to E-450 (C14 Tower Condenser) and is cooled by untreated boiler feed water. Non-condensable vapor is routed to E-451 (C14 Tower Vent Condenser) and is cooled by cooling water.

Explain why two ejector stages (Z-450 and Z-451) are used, and describe the path of the gas stream through them, including any intermediate cooling steps.

Two ejector stages (Z-450 and Z-451) are used to create a deeper vacuum. Gas from D-450 is routed to Z-450 and then cooled in E-459 (C14 Tower Ejector Interstage Condenser) before being routed to Z-451 and finally to E-480.

Describe the flow path of the liquid bottom stream from D-450, specifying the purpose of each unit it encounters before either returning to T-450 or exiting as product.

<p>The liquid bottom stream from D-450 is routed to F-450 (C14 Tower Reflux Strainer). Then, P-450 A/B pumps this stream either back to T-450 as reflux, or to E-452 (C14 Product Cooler) before being sent to TK-814 (C14 Product Tank) as the C14 product.</p> Signup and view all the answers

Explain the purpose of E-455 (C14 Tower Reboiler) and describe the flow path of the liquid and vapor streams associated with it.

<p>E-455 (C14 Tower Reboiler) heats the bottom liquid from T-450 using Dowtherm to create vapor, which is then routed back to T-450 to provide heat and drive separation. The remaining liquid is then sent to T-460 (C16 Tower) as feed.</p> Signup and view all the answers

Flashcards

T-450 (C14 Tower) Function

Separates C14 feed into overhead vapor (C14 Product) and bottom liquid (C16-C24).

E-450 (C14 Tower Condenser)

Cools the T-450 overhead vapor using untreated boiler feed water.

D-450 Role

Receives condensed vapor from E-450 and routes non-condensable vapor to E-451.

E-451 (C14 Tower Vent Condenser)

Cools non-condensable vapor from D-450 using cooling water.

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E-455 (C14 Tower Reboiler)

Heats the T-450 bottom liquid stream using Dowtherm, creating vapor that returns to T-450.

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Study Notes

  • C14-C24 feed from T-440 bottom goes to F-453, then to T-450, separating into C14 overhead vapor and C16-C24 bottom liquid.
  • T-450 overhead vapor is cooled in E-450 using boiler feed water, with condensate going to D-450 and non-condensables to E-451.
  • Cooled overhead gas from D-450, along with non-condensables from E-480, goes to Z-450, then E-459, and Z-451, using 100 psig steam to pull a vacuum.
  • Liquid bottom from D-450 goes through F-450 via P-450A/B back to T-450 as reflux and to E-452 for cooling before storage in TK-814; off-spec C14 goes to Unit 1791.
  • T-450 bottom liquid goes to E-455 for heating with Dowtherm, with the vapor returning to T-450 and the liquid bottom routed by P-455A/B to T-460.

Equipment Details

  • F-453 removes particulate matter from the T-450 feed.
  • T-450 (4’6”D x 81’4”L) separates C14-C24 into C14 overhead product, with C16-C24 blend as feed for T-460.
  • Key process control objectives for T-450 are maintaining C16 concentration in the overhead product and C14 concentration in the bottoms at specification..
  • E-450 cools and condenses T-450 overhead vapor using boiler feed water, providing reflux and C14 product to storage.
  • D-450 (3’6”D x 8’L) separates liquid for reflux and C14 product from non-condensable vapor.
  • E-451 cools and condenses overhead vapor from D-450 using cooling water, to be used as reflux on T-450.
  • Z-450 is the 1st stage ejector installed to lower the pressure of T-450 overhead.
  • E-459 cools and condenses steam from Z-450 using cooling water.
  • Z-451 is the 2nd stage ejector installed to further lower the pressure of T-450 overhead.
  • P-450A/B are 15 HP pumps circulating reflux to T-450 and routing C14 product to TK-814.
  • F-450 removes particulate matter from the T-450 feed.
  • E-452 cools the C14 product with cooling water before storage.
  • E-455 heats T-450 bottoms with Dowtherm, boiling it into vapor; kettle shape provides space for vapor expansion.
  • P-455A/B are 5 HP pumps routing liquid bottom from T-450 to T-460.

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