Laboratory Techniques Flashcards
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Questions and Answers

Apply ___ or ___ to the glass tubing and the rubber stopper when inserting the tubing through the stopper.

water, glycerol

Glassware should always first be cleaned with a soap or detergent using ___ water.

tap

Safety information about any chemical can be obtained from a collection of ___ generally located in the stockroom or at several websites on the internet.

MSDS

In preparing an aqueous solution of a solid in a volumetric flask, always add ___ to the volumetric flask first.

<p>water</p> Signup and view all the answers

The ___ sign is used to identify a potential danger in handling a chemical in this manual.

<p>international caution</p> Signup and view all the answers

Always place ___ or a ___ on the balance pan to measure the mass of a chemical on a balance.

<p>weighing paper, dry container</p> Signup and view all the answers

The mass difference between the mass of the sample and the mass of the weighing paper is called the ___ of the sample.

<p>tared mass</p> Signup and view all the answers

In handling small volumes of solutions, the use of a ___ is the choice of most chemists.

<p>small test tube</p> Signup and view all the answers

A 75-mm (~3 inch) test tube has a volume of about ___ ml.

<p>3</p> Signup and view all the answers

Always use a ___ to assist in the transferring of a solution from one vessel to another.

<p>stirring rod</p> Signup and view all the answers

A precipitate is flushed from a beaker using the solvent contained in a ___.

<p>wash bottle</p> Signup and view all the answers

A bowl of a filter funnel used for gravity filtration should always be kept about ___ full with solution during the filtering process.

<p>1/2 to 1/3</p> Signup and view all the answers

To remove the suction during a vacuum filtration procedure, first ___ and then ___.

<p>disconnect hose, turn off water</p> Signup and view all the answers

A nonluminous flame supplied with a reduced supply of fuel is called a ___ flame.

<p>cool</p> Signup and view all the answers

A test tube should be less than ___ full when heated directly with a 'cool' flame.

<p>1/3</p> Signup and view all the answers

In heating a liquid in a test tube directly with a 'cool' flame, the test tube should be moved in and out of the flame with a circular motion with most of the heating applied at the ___ of the liquid.

<p>top</p> Signup and view all the answers

The reading and recording of a volume of liquid in volumetric glassware should include all digits read directly from the calibration marks on the glassware plus ___.

<p>one uncertain digit</p> Signup and view all the answers

After the buret is filled with titrant, the stopcock should be opened to allow some titrant to drain through the tip. The purpose of this procedure is to ___.

<p>eliminate air bubbles from the tip</p> Signup and view all the answers

A ___ is used to touch a solution to test paper for measuring the acidity/basicity of a solution.

<p>litmus paper</p> Signup and view all the answers

A 'yellow 4' appears on a reagent bottle: 'yellow' refers to the ___ of the chemical and the '4' indicates that the chemical ___.

<p>reactivity, explosive</p> Signup and view all the answers

What does 'Blue' on MSDS mean?

<p>health hazard</p> Signup and view all the answers

What does 'Red' on MSDS mean?

<p>fire hazard</p> Signup and view all the answers

The bottom white symbol on MSDS is left for?

<p>specific hazard</p> Signup and view all the answers

The final step in cleaning glassware is to dry it with a clean paper towel.

<p>False</p> Signup and view all the answers

Glassware is clean if no water droplets cling to its wall.

<p>True</p> Signup and view all the answers

A chemical with a blue hazard label (#3 rating) means that the chemical is highly reactive.

<p>False</p> Signup and view all the answers

To avoid waste in the use of chemicals, always return the unused portion directly to the original reagent bottle.

<p>False</p> Signup and view all the answers

If you are uncertain as to how to dispose of a chemical after use, dumping it into the sink, followed by a flush with copious amounts of water, is always a safe disposal procedure.

<p>False</p> Signup and view all the answers

Most laboratory balances in the general chemistry laboratory can measure the mass of a substance to less than 0.01g.

<p>False</p> Signup and view all the answers

Water-soluble gases can be collected by water displacement.

<p>False</p> Signup and view all the answers

Use a spatula to transfer chemicals from a reagent bottle.

<p>False</p> Signup and view all the answers

Never lay the stopper from a liquid reagent bottle on the laboratory bench.

<p>True</p> Signup and view all the answers

Two equal folds are used to prepare a piece of circular filter paper from a funnel.

<p>True</p> Signup and view all the answers

The funnel stem of a filter funnel should touch the side of the receiving flask during the filtering procedure.

<p>True</p> Signup and view all the answers

The minimum number of centrifuge tubes that should be placed into a centrifuge during its operation is two.

<p>True</p> Signup and view all the answers

Given a choice, always use a fume hood in lieu of an improvised hood.

<p>True</p> Signup and view all the answers

The heat source for heating and evaporating flammable liquids should be a hot plate.

<p>True</p> Signup and view all the answers

The thumb is the digit of choice in controlling the dispensing of a liquid from a pipet.

<p>False</p> Signup and view all the answers

A pipet should be rinsed several times with the liquid or solution before it is finally filled.

<p>True</p> Signup and view all the answers

Blow out the solution remaining in the pipet tip after the solution has drained from the pipet.

<p>False</p> Signup and view all the answers

Always read the bottom of the meniscus for a liquid in glassware.

<p>True</p> Signup and view all the answers

Use a collapsed rubber pipet bulb to draw liquid into a pipet.

<p>True</p> Signup and view all the answers

A buret must always be filled to the top (the zero mark) before every titration procedure.

<p>False</p> Signup and view all the answers

After the endpoint is reached in a titration, the volume of titrant should be read immediately.

<p>False</p> Signup and view all the answers

A half-drop of titrant can be dispensed from a buret.

<p>True</p> Signup and view all the answers

A good chemist, without reservation, smells all chemicals.

<p>False</p> Signup and view all the answers

Acids cause litmus paper to appear red.

<p>True</p> Signup and view all the answers

Litmus paper should be placed directly into the test solution to determine its acidity/basicity.

<p>False</p> Signup and view all the answers

Study Notes

Laboratory Techniques

  • To ease the insertion of glass tubing into a rubber stopper, apply water or glycerol to both.
  • Always clean glassware first with soap or detergent using tap water.
  • Safety information for chemicals can be found in Material Safety Data Sheets (MSDS), available in stockrooms or online.
  • When preparing an aqueous solution in a volumetric flask, start by adding water first.
  • The international caution sign indicates potential dangers in chemical handling.
  • Use weighing paper or a dry container when measuring chemical mass on a balance.
  • The tared mass of a sample is the mass difference between the sample and the weighing paper.
  • Small test tubes are the preferred choice for handling small volumes of solutions.
  • A standard 75-mm test tube can hold approximately 3 ml of liquid.
  • Always use a stirring rod to transfer a solution between vessels.
  • A wash bottle is utilized for flushing precipitates from beakers with solvent.
  • During gravity filtration, a filter funnel's bowl should remain half to one-third full of the solution.
  • For vacuum filtration, disconnect the hose and turn off the water to remove suction safely.
  • A cool flame has a reduced fuel supply and is used for specific heating tasks.
  • Test tubes heated directly with a cool flame should be filled to less than one-third of their capacity.
  • Move the test tube in and out of the cool flame with a circular motion, applying heat primarily to the liquid's top.
  • Record liquid volumes in volumetric glassware including all digits from calibration marks and one uncertain digit.
  • To eliminate air bubbles, allow some titrant to drain from the buret tip after filling it.
  • Litmus paper is used to test the acidity or basicity of a solution.
  • The color coding on reagent bottles indicates reactivity and hazard levels, e.g., "yellow 4" signifies explosive reactivity.
  • Blue on an MSDS indicates a health hazard, while red indicates a fire hazard.
  • The bottom white symbol on an MSDS is reserved for specific hazards.
  • Cleaning glassware concludes with evaporation rather than drying with paper towels.
  • Glassware is considered clean if no water droplets cling to its walls.
  • A blue hazard label (#3 rating) does not imply high reactivity; yellow indicates reactivity.
  • Unused chemicals should not be returned to the original reagent bottle; share excess with other chemists instead.
  • Never dispose of chemicals by dumping them in the sink; follow proper procedures and instructions.
  • General chemistry balances can measure mass to 0.01 g, but not less.
  • Water-soluble gases should not be collected using the water displacement method; it is only effective for water-insoluble gases.
  • Using a spatula to transfer chemicals from a reagent bottle is discouraged.
  • Do not place liquid reagent stoppers on the laboratory bench.
  • Two equal folds are sufficient to prepare circular filter paper for a funnel.
  • Ensure the funnel stem of a filter funnel touches the side of the receiving flask during filtering.
  • At least two centrifuge tubes should be used when operating a centrifuge for balance.
  • Always prefer using a fume hood over makeshift hoods in laboratory settings.
  • A hot plate is the recommended heat source for evaporating flammable liquids.
  • Control the dispensing of liquid from a pipet using the forefinger, not the thumb.
  • Rinse a pipet multiple times with a solution before filling it for accurate measurements.
  • Do not blow out the remaining liquid in a pipet tip after draining; it is accounted for in calibration.
  • Always read the bottom of the meniscus when measuring liquids in glassware.
  • Use a collapsed rubber pipet bulb for drawing liquid into a pipet.
  • A buret should not be filled to the top before titration; instead, it should be filled just below the zero mark.
  • Read the buret volume after 10-15 seconds post-titration to ensure accuracy.
  • A half-drop of titrant can indeed be dispensed from a buret.
  • Chemists should not smell all chemicals indiscriminately; only do so when safe and necessary.
  • Acids turn litmus paper red, while bases turn it blue.
  • Litmus paper should not be directly immersed into the test solution; instead, use a stirring rod that has been in contact with the solution first.

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Test your knowledge of essential laboratory techniques with these flashcards. Each card focuses on important terms and definitions related to safety and equipment handling in a laboratory setting. Perfect for students and professionals looking to refresh their knowledge.

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