Biodiesel Reactor Design and Performance Test
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Questions and Answers

What is the optimal temperature range for biodiesel production to ensure methanol has not reached its boiling point?

  • 65 °C to 70 °C
  • 70 °C to 75 °C
  • 55 °C to 60 °C
  • 60 °C to 65 °C (correct)

What role do agitation and baffles play in the biodiesel reactor?

  • They contribute to the homogenity of temperature. (correct)
  • They increase the boiling point of methanol.
  • They reduce the overall reaction time.
  • They cool down the reactor contents.

At what RPM agitation does the temperature within the biodiesel reactor achieve homogeneity?

  • 200 rpm and 300 rpm
  • 100 rpm and 200 rpm (correct)
  • 50 rpm and 150 rpm
  • 300 rpm and 400 rpm

What is the standard deviation value of temperature variation in the biodiesel reactor?

<p>0 °C to 0.25 °C (D)</p> Signup and view all the answers

Which statement accurately describes the importance of temperature in the biodiesel production process?

<p>Temperature influences the reaction rate and must be carefully controlled. (C)</p> Signup and view all the answers

What phenomenon occurs due to the insertion of baffles in large-scale reactor tanks?

<p>Increased temperature uniformity (D)</p> Signup and view all the answers

What is the significance of measuring temperature at three positions in the biodiesel reactor?

<p>To verify the temperature uniformity throughout the reactor. (A)</p> Signup and view all the answers

What is necessary for ensuring that the biodiesel reaction takes place entirely within the reactor?

<p>Homogenous temperature distribution (C)</p> Signup and view all the answers

What process is described for producing biodiesel?

<p>Transesterification of oil and methanol (A)</p> Signup and view all the answers

At what rpm was the total glycerol content of biodiesel within the acceptable Indonesian standard?

<p>100 rpm (A)</p> Signup and view all the answers

Which temperature range is indicated for the acid value of biodiesel from all treatments?

<p>&lt; 0.4 mg KOH/g (B)</p> Signup and view all the answers

What was the yield percentage of biodiesel at 1000 rpm?

<p>80% (B)</p> Signup and view all the answers

How does temperature influence the quality of biodiesel production during transesterification?

<p>Temperature must be optimal for reaction efficiency. (B)</p> Signup and view all the answers

What pattern was observed regarding biodiesel yield across various experiments?

<p>No special pattern was observed. (B)</p> Signup and view all the answers

What was the range of the acid values for biodiesel across all treatments, except at 1000 rpm?

<p>0.06 mg KOH/g to 0.12 mg KOH/g (D)</p> Signup and view all the answers

What was the total glycerol content across all treatments on average?

<p>0.28% (C)</p> Signup and view all the answers

What temperature range was maintained during the biodiesel production process?

<p>60 oC to 65 oC (A)</p> Signup and view all the answers

Which method was used to purify the biodiesel after the transesterification reaction?

<p>Wet washing (B)</p> Signup and view all the answers

What is indicated as the desirable pH value for the wastewater to confirm the removal of catalyst from biodiesel?

<p>7 (A)</p> Signup and view all the answers

At what time duration is the transesterification reaction assumed to be completed?

<p>60 minutes (B)</p> Signup and view all the answers

How was the methyl ester content of biodiesel measured?

<p>By saponification value analysis (A)</p> Signup and view all the answers

What capacity does the reactor tank used for biodiesel production have?

<p>5 L (B)</p> Signup and view all the answers

What component of the reactor is responsible for maintaining the temperature during biodiesel production?

<p>Electric heater (C)</p> Signup and view all the answers

Which of the following components is NOT included in the design of the biodiesel reactor?

<p>Paddle wheel (D)</p> Signup and view all the answers

Flashcards

Biodiesel Reactor

A cylindrical reactor designed for biodiesel production.

Agitator

A device (like a helical screw) that mixes the liquid in the reactor.

Reactor Temperature

The temperature of the liquid within the reactor; important for the reaction and product quality during biodiesel production.

Optimal Temperature

The best temperature range (60-65°C) for biodiesel production, where methanol isn't boiling.

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Homogenous Temperature

A consistent temperature throughout the liquid in the reactor to ensure a complete reaction.

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Agitation (RPM)

The rate of stirring (revolutions per minute) that affects temperature distribution within the reactor.

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Temperature Distribution

Measuring temperature at different locations (top, middle, bottom) within the reactor to see if it's the same throughout.

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Standard Deviation

Measures how spread out the temperature measurements are; a small standard deviation indicates a homogenous temperature.

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Standard Deviation of Liquid Temperature

A measure of the variability or spread of liquid temperature during agitation, as shown in Figure 5.

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Temperature Distribution in Reactor

The variation in liquid temperature across the reactor at different agitation rates, illustrated with Figure 6

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Biodiesel Quality Standard

Standards, like SNI 7182:2015, used to measure biodiesel quality.

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Total Glycerol

A parameter to evaluate biodiesel quality, values should be below 0.24% (in this study).

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Acid Value

Measurement of acidity in biodiesel, should be less than 0.4 mg KOH/g.

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Biodiesel Yield

The percentage of biodiesel produced in the transesterification reaction.

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Optimal Agitation Speed

The agitation speed that maximizes processes efficiency and biodiesel yield.

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Transesterification Reaction

Chemical reaction between oil and methanol to produce biodiesel

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Biodiesel Production Temperature

The temperature of the liquid during biodiesel production was maintained between 60°C and 65°C.

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Agitation Rotation Values

The experiment used 10 different agitation speeds (rotations per minute) ranging from 100 rpm to 1000 rpm.

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Transesterification Time

The transesterification reaction was assumed to be complete in 60 minutes.

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Glycerol Separation Method

Biodiesel was separated from glycerol by a sedimentation process.

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Catalyst Removal Method

The catalyst was removed from the biodiesel using a wet washing method with warm water (60°C).

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Neutralization Check

The pH of the wastewater was measured to ensure no catalyst remained in the biodiesel (a neutral pH of 7).

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Biodiesel Quality Tests

The quality of the biodiesel was checked by measuring saponification number, glycerol total, acid value, yield, and methyl ester content.

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Methyl Ester Content Measurement

Methyl ester content was measured using saponification value analysis.

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Study Notes

Biodiesel Reactor Design and Performance Test

  • A biodiesel reactor model using a helical screw agitator and baffles was designed.
  • The helical screw type was chosen for its ability to agitate viscous liquids with low energy, while baffles were used to create uniform mixing.
  • The research aimed to produce a biodiesel reactor model and determine the optimal operating parameters for biodiesel production.
  • A cylindrical biodiesel reactor with a height of 300mm and a diameter of 168mm was used.
  • The helical screw agitator had four screws and four baffles were installed along the reactor's wall.
  • Biodiesel was produced using a catalytic method with a 1.5% w/w KOH catalyst at temperatures ranging from 60°C to 65°C for 60 minutes.
  • The saponification value analysis showed that the biodiesel contained 99% w/w methyl ester.
  • The optimal operating conditions for biodiesel production were achieved at 100 rpm, meeting the quality standards and minimizing energy consumption.

Methodology

  • Materials and apparatus were divided into two categories: design and performance testing.
  • Design materials included stainless steel, hollow iron, electric welding machine, grindstone, drilling machine, lathe, etc.
  • Performance testing materials included palm oil, methanol, KOH, phenolphtalein indicator, chemical glassware, and an electrical balance.

Reactor Design

  • The reactor consisted of a cylindrical reactor, helical screw agitator, four baffles, an electric heater, motor, temperature controller, motor rotational speed controller, and a cantilever/frame.
  • The cylindrical reactor had a diameter of 168 mm and a height of 300 mm.
  • The helical screw agitator contained four blades.
  • The baffles were installed along the reactor's walls.
  • The electric heater was located below the agitator.
  • The dimensions of the reactor's components are described in tables.

Performance Test

  • Liquid temperature distribution within the reactor was measured at different speeds and locations.
  • The optimal temperature range for the transesterification reaction was 60-65°C.
  • The results showed that the helical screw agitator and baffles effectively mixed the reactants at a high yield (ranging from 80-92%) without variation as the speed increased.
  • Standard deviation values of liquid temperatures were low with variation of 0 °C to 0.25°C, demonstrating uniform temperatures.
  • All treatments had total glycerol of 0.28%, except at 100 rpm, which had 0.12%. (values below 0.24% are preferred)

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Description

Explore the design and performance testing of a biodiesel reactor featuring a helical screw agitator. This quiz covers the optimal parameters for biodiesel production, including catalyst use, temperature control, and energy efficiency. Test your understanding of the methods employed in producing high-quality biodiesel.

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