Tanecik Teknolojisi: Particle Science

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Questions and Answers

Which of the following is considered an 'Esas Özellik (Measurable Property)' of particles?

  • Specific surface area
  • Settling velocity
  • Particle size (correct)
  • Bulk density

A researcher is analyzing a powder sample. Which particle size range would be classified as a colloidal solution?

  • Greater than 1 mm
  • Less than 1 nm
  • 1 - 1000 nm (correct)
  • Greater than 1000 nm

In particle technology, what distinguishes a suspension from a true solution and a colloidal solution?

  • Particle size and homogeneity (correct)
  • Only particle size
  • Electrical charge and stability
  • Only homogeneity

When preparing a lab report, which of the following sections is expected to contain a discussion on the accuracy and precision of the measurements?

<p>Results and discussion (B)</p> Signup and view all the answers

Why is particle size considered an important characteristic to monitor throughout a mineral processing procedure?

<p>It affects every stage of the process, from selection to environmental conditions (D)</p> Signup and view all the answers

Which particle shape descriptors is defined as the ratio of the length of Feret's diameter perpendicular to Feret's diameter divided by Feret's diameter?

<p>Aspect Ratio (D)</p> Signup and view all the answers

What is indicated if a material settles quickly in a fluid?

<p>High density and large particle size. (C)</p> Signup and view all the answers

What would be the best next step per Student Lab safety guidelines?

<p>Clean the equipment used in the lab (C)</p> Signup and view all the answers

A material consisting of solid particles is dispersed in a liquid, such as clay in water. What term BEST describes this type of system?

<p>Suspension (D)</p> Signup and view all the answers

Which method is most suitable for measuring the size of particles with a diameter of approximately 500 micrometers?

<p>Sieve analysis (A)</p> Signup and view all the answers

The particle size of the powder used in a tablet formulation affects its dissolution rate. Which of the following methods is most likely used to determine the particle size distribution?

<p>Laser diffraction (A)</p> Signup and view all the answers

A researcher is tasked with rapidly determining the particle size distribution of a large batch of granular material. Which method would be most appropriate?

<p>Sieve analysis (D)</p> Signup and view all the answers

Which is a valid application of particle technology in mining?

<p>Ore refinement (C)</p> Signup and view all the answers

What is 'Feret's diameter' used to measure?

<p>Irregular particle size (A)</p> Signup and view all the answers

What is the formula for sphericity?

<p>(4 pi * da / p^2) * 100 (C)</p> Signup and view all the answers

If all other factors are constant, how does increased viscosity affect the settling velocity of particles in a fluid?

<p>Decreases settling velocity (B)</p> Signup and view all the answers

In the context of sampling and particle size determination, what does 'representative sampling' ensure?

<p>The sample accurately reflects the properties of the entire batch (C)</p> Signup and view all the answers

Which type of system is most likely described by the following: 'Toz, duman'?

<p>Gas - Solid (A)</p> Signup and view all the answers

In comminution, how does Liberation Step enable Separation Step?

<p>By physically exposing valuable minerals through size reduction (C)</p> Signup and view all the answers

During a particle size analysis using sieving, a student observes that a significant portion of the sample is retained on the finest sieve. What does this indicate?

<p>The material contains a high proportion of fine particles (B)</p> Signup and view all the answers

For irregularly shaped particles, which of the following statements best describes the statistical diameters?

<p>They are averages taken at consistent angles from the particle. (B)</p> Signup and view all the answers

What is the primary purpose of a 'technical visit'?

<p>To provide students with practical, real-world industry exposure (C)</p> Signup and view all the answers

In the context of particle technology, what is the 'liberation size'?

<p>The particle size required to achieve complete separation of valuable minerals from waste (D)</p> Signup and view all the answers

When is the 'ARA TATIL' period for the Tanecik Teknolojisi(Particle Technology) course?

<p>April 1 (A)</p> Signup and view all the answers

If a sample of particles is described as having a high 'aspect ratio', what can be inferred about the particle's shape?

<p>The particles are elongated or needle-like (A)</p> Signup and view all the answers

Which expression is correctly describing the relationship between elek capi and Stokes'a cap?

<p><code>dst = dA *0.94</code> (A)</p> Signup and view all the answers

Which factor has the highest impact on processes that require the suspension of solid particles in a liquid?

<p>The surface charge of the particles (A)</p> Signup and view all the answers

What is one factor that students must keep in mind when at the lab?

<p>Students must participate in cleaning experimental equipments after using it. (B)</p> Signup and view all the answers

A research team is investigating the suitability of a novel material for use in a catalytic converter. Which particle properties are most critical for this application?

<p>Surface area and porosity (C)</p> Signup and view all the answers

A food scientist is studying the texture of a powdered milk product. Which particle characteristic most directly influences the product's flowability and dispersibility?

<p>Particle shape (B)</p> Signup and view all the answers

During the Tanecik Teknolojisi course, students are required to prepare a presentation on their homework. When will students do this?

<p>Presentations will be held on May 27 (A)</p> Signup and view all the answers

In ore refinement, what happens during Size Reduction?

<p>Comminution (D)</p> Signup and view all the answers

Which of the following is an example of a system where gas is dispersed in a liquid?

<p>Soap foam (D)</p> Signup and view all the answers

Which are the responsibilities of students that attend lab experiments?

<p>Maintaining general cleanliness and hygiene. (A)</p> Signup and view all the answers

In a research context, can particle size and particle shape be used interchangeably?

<p>False (B)</p> Signup and view all the answers

Which device would be most helpful to determine the shape factor of a material?

<p>Image Analysis (A)</p> Signup and view all the answers

During sedimentasyon, what is assumed when calculating average particle size?

<p>Particles are smooth and spherical (A)</p> Signup and view all the answers

In Tanecik Teknolojisi (Particle Technology), which topic does one NOT need to include in their homework?

<p>Social Impact (A)</p> Signup and view all the answers

Which of the following is NOT a valid categorization of particle sizes?

<p>Foam (A)</p> Signup and view all the answers

Which concept aims to categorize the different sizes of particles?

<p>Particle Classification (C)</p> Signup and view all the answers

Flashcards

Parça Sistemi

A solid, liquid, or gas in which small pieces of another material are dispersed.

Parça Boyutuna Göre Sınıflandırma

A way to group particles by their size, such as true solutions, colloidal solutions, and suspensions.

Tane Boyutu

The range of dimensions of individual particles in a collection.

Stokes Çapı

The diameter of a sphere that falls at the same rate as the irregular particle.

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Mikron

A measurement equal to one millionth of a meter.

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Martin Çapı

The smallest diameter of a particle when viewed under a microscope.

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Feret Çapı

The maximum horizontal distance across a particle.

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Elek Çapı

Screens used to separate particles by size.

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Tanecik Özellikleri

Essential and derived characteristics of individual pieces of matter.

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Parça Boyutunun Önemi

The use of particle size and shape to isolate valuable minerals.

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Study Notes

  • Tanecik Teknolojisi is the study of particle Science
  • Presented by Prof. Dr. Gülay BULUT and Dr. Öğretim Üyesi Ş. Beste AYDIN
  • At İTÜ; Maden Fak. Cevher Hazırlama Müh. Bölümü
  • For the 2024-2025 Spring Term

Course Schedule

  • Spring Semester runs from February 17 to May 30
  • Final Exams held between June 10-23
  • Classes are on Tuesdays from 08:30 to 12:30

Key Topics

  • Introduction to particulate materials
  • Average particle sizes in particulate materials
  • Shape factor and determination
  • Density, bulk density, and determination of bulk weight
  • Evaluation of size measurements and measurement methods
  • Frequency distribution-histogram, normal distribution, log normal distribution
  • Surface properties and specific surface area of particulate material
  • Motion of solid particles in fluid medium and measurement methods based on hydrodynamic similarities
  • Behavior of solid particles in fluid medium in ore dressing applications

Laboratory Applications

  • Includes shape factor determination
  • Image analysis
  • Specific surface area and size analysis
  • Sieve and Malvern devices
  • Determination of bulk and true density plus settling/Andreasan pipette methods

Assessment

  • Year-end exam: 50%
  • Year-round activities: 50%
  • Two short exams: 5% each
  • Year-round exam: 10%
  • Lab application: 20%
  • Term project-homework: 10%

Homework

  • Homework assignments are compulsory
  • Topics are distributed to students on February 25
  • Assignments should be 10-20 pages long, submitted to Prof. Dr. Gülay BULUT by May 27, 2025
  • Students do a 20-25 minute PowerPoint presentation on the same day

Homework Topics

  • Fritsch particle size measuring device
  • Image analysis device and size distribution functions
  • Surface properties and measurement methods of particulate material (SH+LIN+BET)
  • Specific weight and measurement methods (TSE, reserve, and bulk-oriented measurements)
  • Grain size measurement methods
  • Importance and measurement methods of shape factor in particulate material
  • Screening and distribution functions (GGS and RRB)
  • Applications of solid particles in fluid in ore enrichment processes
  • Measurement methods of fluid-borne fine-sized particles (sedimentation, Andreasen pipette, etc.)
  • Segregation events encountered in particulate material
  • Standards used in particle technology
  • Importance of particulate materials in terms of human health
  • Pore, porosity, measurement methods
  • Comparison of particle measurement methods
  • Nanotechnology in ore preparation
  • Importance of particle properties in ore preparation

Lab Rules

  • Halide Dursun is responsible for the practical studies of the Particle Technology course
  • Each application is carried out in laboratories of the Ore Dressing Engineering department
  • Attending lab sessions is compulsory, lab coats must be worn
  • Eating, smoking and drinking is prohibited
  • Attendee's must ensure equipment is cleaned under supervision
  • Individual reports must be prepared for each practical, to be submitted to experiment supervisors by specified dates
  • Each student is entitled to only one make-up experiment

Report Writing

  • Introduction
  • Experiment related info
  • Experimental studies including apparatus, method, procedure, results, and discussion
  • General results
  • References

Technical Visit

  • There are plans for a 1-day technical trip to the Eczacıbaşı-Esan research center in Gebze

Topic: Particle Technology General Definitions, Particle Size

  • Focuses on the dynamics, shape, size distributions, and measurement.
  • Discusses surface area, sludge, slurry, and transport in fluid mechanics.
  • Covers fine grinding and sampling, with importance of grain properties in transport, storage, sizing, enrichment, and waste
  • Explores particle vs. granular material, system, the definition, and characterization

Definitions

  • Particle
  • Grain
  • Particulate Material
  • Particulate System
  • Particulate Material Properties

Particulate System and Phase

  • Solid can exist in solid-liquid-gas
  • Liquid can exist in solid-liquid-gas
  • Gas can exist in solid-liquid

Examples by Dispersed Phase

  • Solid in solid: Granular like ores
  • Solid in liquid: Suspension
  • Solid in gas: Dust
  • Liquid in solid: Not provided
  • Liquid in liquid: Emulsions of water and oil
  • Liquid in gas: mist/fog
  • Gas in solid: Closed pores
  • Gas in Liquid: Air bubbles

Examples Using an Alternative Approach

  • Liquid as the dispersing medium: dyes and liquid gold
  • Liquid as the dispersed phase: milk
  • Liquid as the medium when gas is dispersed: whipped cream
  • Solid is medium with dispersed solids: alloys
  • Solids as dispersing medium and liquid dispersed: jellies
  • Solids as dispersing medium with a dispersed gas: volcanic rock
  • Gas as a medium with dispersed solid: dust
  • Gas as a medium with a dispersed liquids: clouds

Particle Size Classification

  • Particle size is categorized based on dimensions relative to true solutions, colloidal solutions, and suspensions
  • True solutions feature particles less than 10⁻⁷ cm
  • Colloidal solutions involves particles between 10⁻⁷ cm and 10⁻⁵ cm
  • Suspensions consist of particles larger than 10⁻⁵ cm

Classifying solutions by particle size

  • True solutions have particle sizes under 1 nm
  • Colloidal solutions range from 1 to 1000 nm
  • Suspensions exceeding 1000 nm

Mixtures

  • True solutions are homogenous, and colloidal and suspensions are heterogenous

Filterability

  • True solutions pass rapidly through filter paper
  • Colloidal solutions pass through filter paper but not parchment paper
  • Suspensions cannot pass through either type of paper

Visibility

  • Particles in true and colloidal solutions are imperceptible without advanced microscopes
  • Suspension particles are visible to the naked eye

Appearance

  • True solutions are transparent
  • Colloidal are semi-transparent
  • Suspensions are matte

Granularity

  • Ranges from atomic to macroscopic
  • Atomic particles such as atoms, molecules
  • Macroscopic examples include sand and crushed rock

Particle Size in Microns

  • Fine sand ranges from 20-200
  • Hair has a diameter of 100
  • Clouds have 30
  • Red blood cells are 8
  • Clay is less than 2
  • Cigarette smoke is less than 2
  • Bacteria ranges from 0.2-40
  • Viruses are less than 0.5
  • Silt is between 2-20

Particle Shape

  • Size include large and small
  • Shape include round and flat
  • Surface properties include Smooth and rough

Particle Properties

  • Essential properties are measurable
  • Secondary properties are calculated

Essential Measurable Properties

  • Includes size, shape, composition, structure

Secondary Calculated Properties

  • Includes settling velocity, bulk density and specific surface area

Particle (Grain) Size

  • Various diameters are measured, and include:
  • Stokes or settling diameter
  • Surface to Volume
  • Sieve
  • Projected area
  • Feret
  • Volume Diameter.

Particle Size in Ore Treatment has importance in

  • Choosing the right method and equipment
  • Monitoring equipment performance
  • Meeting market conditions
  • Ensuring safety for workers and environment

Tane Boyutunun Önemi

Particle types and measurement

  • Regular shapes have easily measured dimensions
  • Irregular shapes are measured with three group dimensions as per(Svarovsky, 1977):
  • Equivalent sphere
  • Equivalent circle
  • Statistical diameters

Sphere Diameters

  • Includes calculation of volume, surface area and combined surface area
  • Can also measure Stokes, Newton or Drag effect

Stokes’ Diameter

  • This is a measure or a particles behavior when in a fluid

Equivalent Circle Diameters Include

  • Projected Area
  • Circumference

Statistical Diameters Include

  • Martin
  • Feret
  • Feret Average
  • Length and width
  • Aspect ration
  • Orientation
  • Form factore and perimeter
  • Projected area and perimeter

Diameter Conversion

  • Conversions between different diameters are possible using conversion factors

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