Redox Titration: Iodometry Experiment
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Questions and Answers

The standard solution employed in most iodometric processes is ______ thiosulfate.

sodium

Potassium ______ is an example of a primary standard strong oxidizing agent.

iodate

The commercial H2O2 can be titrated by ______ method.

iodometric

The volume numbers of H2O2 correspond to the amount of available ______.

<p>H2O2</p> Signup and view all the answers

A 10-volume solution will be about ______ % H2O2 by weight.

<p>3</p> Signup and view all the answers

Weigh approximately ______ g of Na2S2O3.5H2O and dissolve in distilled water.

<p>6.24</p> Signup and view all the answers

Weigh 2 g of ______ into a 100 mL beaker.

<p>potassium iodide</p> Signup and view all the answers

Add a few mL of ______ water and swirl for a few minutes until iodine is dissolved.

<p>distilled</p> Signup and view all the answers

Weigh 0.25 g of ______ starch and add it to 50 mL of near boiling water.

<p>soluble</p> Signup and view all the answers

Dissolve a single tablet in 200 mL of ______ water.

<p>distilled</p> Signup and view all the answers

Strain the juice through ______ to remove seeds and pulp.

<p>cheesecloth</p> Signup and view all the answers

Cut a 100 g sample into small pieces and grind in a ______ and pestle.

<p>mortar</p> Signup and view all the answers

Alcohol may remove _______________ from skin and cleaners are available for fabric stains.

<p>stains</p> Signup and view all the answers

Vitamin C, or _______________, is a water-soluble antioxidant that plays a vital role in protecting the body from infection and disease.

<p>ascorbic acid</p> Signup and view all the answers

The concentration of the prepared iodine solution can be more accurately determined by titration with a standard solution of _______________ or a standard solution of potassium thiosulfate using a starch indicator.

<p>ascorbic acid</p> Signup and view all the answers

Ascorbic acid is susceptible to _______________ by atmospheric oxygen over time.

<p>oxidation</p> Signup and view all the answers

If the samples have to be prepared several hours earlier, oxidation can be minimized by the addition of a small amount of _______________ acid.

<p>oxalic</p> Signup and view all the answers

Identification of the endpoint in this titration is significantly affected by the _______________ of the sample solution used.

<p>coloration</p> Signup and view all the answers

For strongly colored juices there can be a problem with the ______ and it is advised to carry out a “rough” titration in order to become familiar with any distinct color change which occurs at the ______.

<p>endpoint endpoint</p> Signup and view all the answers

This will also help by establishing an approximate volume of ______ solution required.

<p>iodine</p> Signup and view all the answers

The above method may be used to carry out a number of interesting investigations regarding the concentration of ______ C in various foods and drinks:

<p>Vitamin</p> Signup and view all the answers

Centre photo: At the ______ all the ascorbic acid has reacted, and the excess ______ reacts with the starch indicator to give a pale blue color.

<p>titration endpoint iodine</p> Signup and view all the answers

Figure 2 shows a ______ of commercial fruit juice.

<p>photograph</p> Signup and view all the answers

Left photo: before ______, added iodine reacts with ascorbic acid leaving the solution colorless.

<p>endpoint</p> Signup and view all the answers

The Left flask, before the endpoint, the color of the solution reflects the pale-yellow color of the ______ juice.

<p>fruit</p> Signup and view all the answers

In the Centre flask, at the titration endpoint all the ascorbic acid has reacted, and any excess iodine reacts with the ______ indicator to form a dark blue-black complex.

<p>starch</p> Signup and view all the answers

Figure 3 illustrates the titration of ______ juice.

<p>orange</p> Signup and view all the answers

Figure 4 illustrates the titration of ______ capsicum.

<p>red</p> Signup and view all the answers

The Centre flask, once all the ascorbic acid has been oxidized, a slight excess of added iodine complexes with the ______ indicator, giving the solution a green colour in this case.

<p>starch</p> Signup and view all the answers

The Right flask, if further iodine solution were to be added, the solution's green colour would become darker as shown, due to the formation of further iodine-______ complex.

<p>starch</p> Signup and view all the answers

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