Proximate Analysis and Energy Content Estimation

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Questions and Answers

What is the moisture content (% weight, wet basis) of the waste sample?

  • 85%
  • 14% (correct)
  • 16.28%
  • 6.25%

After drying at 105°C, the sample is placed in a closed crucible at 950°C. What does the weight loss in this step primarily represent?

  • Volatile combustible matter (correct)
  • Ash content
  • Fixed carbon
  • Moisture content

What is the volatile combustible matter (% weight) of the waste sample?

  • 8%
  • 73% (correct)
  • 87%
  • 13%

The fixed carbon content is determined by heating the sample in an open crucible at 950°C.

<p>False (B)</p> Signup and view all the answers

What is the ash content (% weight) of the waste sample?

<p>5% (A)</p> Signup and view all the answers

Which heating step directly determines the ash content?

<p>Heating in an open crucible at 950°C</p> Signup and view all the answers

The difference between the dry sample weight and weight after heating in a closed crucible represents the ______ content.

<p>volatile combustible matter</p> Signup and view all the answers

Calculated by difference, what is the fixed carbon content (% weight) of the waste sample?

<p>17% (D)</p> Signup and view all the answers

Match the analysis step with the component it primarily measures:

<p>Drying at 105°C = Moisture content Heating in a closed crucible at 950°C = Volatile combustible matter Heating in an open crucible at 950°C = Ash content</p> Signup and view all the answers

What is required to estimate the energy content (in kcal/kg) using an empirical equation?

<p>Proximate analysis data (moisture, volatile matter, fixed carbon, ash)</p> Signup and view all the answers

Flashcards

Moisture Content (Dry Basis)

The percentage of weight lost when heating a sample at 105°C until it reaches a stable weight. Calculated as ((Initial Weight - Dry Weight) / Dry Weight) * 100.

Volatile Combustible Matter

The percentage of weight lost when heating a dry sample in a closed crucible at 950°C. Calculated as ((Dry Weight - Crucible Weight) / Initial Weight) * 100.

Ash Content

The percentage of weight remaining after heating the sample in an open crucible at 950°C, allowing complete combustion. Calculated as (Ash Weight / Initial Weight) * 100

Fixed Carbon

Calculated by subtracting the percentages of moisture, volatile combustible matter, and ash content from 100%. Represents the carbon that remains after volatiles are driven off.

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Energy Content Estimation

An empirical estimate of the energy content (in kcal/kg) of waste derived from its proximate analysis. The specific equation was not given in the document.

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Study Notes

  • A proximate analysis was conducted on a 100g waste sample
  • The sample was placed in a 105°C oven until a stable weight of 86g was achieved

Moisture Content

  • The moisture content is calculated on a dry basis
  • Original weight: 100g
  • Weight after drying: 86g
  • Moisture content: [(100g - 86g) / 86g] * 100% = 16.28%

Volatile Combustible Matter

  • The dried sample (86g) was placed in a closed crucible at 950°C
  • Weight after baking in closed crucible: 13g
  • Volatile combustible matter: [(86g - 13g) / 86g] * 100% = 84.88%

Fixed Carbon

  • The sample was then placed in an open crucible and baked at 950°C
  • Weight after baking in open crucible: 5g
  • Fixed carbon: [(13g - 5g) / 86g] * 100% = 9.30%

Ash Content

  • Weight after baking in open crucible: 5g
  • Ash content: (5g / 86g) * 100% = 5.81%

Energy Content Estimation

  • The values obtained from the proximate analysis can be used to estimate energy content using empirical equations
  • This requires the specific equation, which isn't provided, so energy content cannot be calculated

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