Laboratory Recovery of Flammable Residues
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Questions and Answers

What is the purpose of comparing the chromatographic pattern of an unknown sample to known petroleum products?

  • Determining the explosive nature of the unknown sample
  • Identifying the source of the unknown sample (correct)
  • Assessing the color of the unknown sample
  • Measuring the density of the unknown sample

Where can a forensic analyst find a searchable library to compare the chromatograms of accelerant standards?

  • Local library archives
  • Forensic journal articles
  • Chemistry textbooks
  • ILRC website (correct)

What technique can simplify complex chromatographic patterns in forensic analysis?

  • Gas chromatography/mass spectrometry (correct)
  • Column chromatography
  • Paper chromatography
  • Thin-layer chromatography

What is the characteristic nature of explosives that distinguishes them from other substances?

<p>Rapid oxidation reaction (B)</p> Signup and view all the answers

Which of the following is an example of a low explosive used widely?

<p><strong>Black powder</strong> (A)</p> Signup and view all the answers

What is the term for the speed of decomposition exhibited by low explosives confined to containers?

<p><strong>Deflagration</strong> (C)</p> Signup and view all the answers

What is the purpose of placing a charcoal strip in the airtight debris container during heating?

<p>To absorb much of the vapors for recovery of accelerant residues. (A)</p> Signup and view all the answers

How are the volatile residues in fire-scene debris trapped during the laboratory recovery process?

<p>By heating the airtight container and capturing the vapor in its airspace. (D)</p> Signup and view all the answers

Why is a syringe used after heating the container during laboratory recovery of flammable residues?

<p>To remove the trap vapor for injection into a gas chromatograph. (B)</p> Signup and view all the answers

What role does the solvent play in the vapor concentration technique?

<p>Recovering accelerant vapors absorbed by a charcoal strip. (D)</p> Signup and view all the answers

Why is gas chromatography considered a sensitive and reliable instrument for detecting and characterizing flammable residues?

<p>It separates hydrocarbon components and produces characteristic chromatographic patterns. (B)</p> Signup and view all the answers

How can a forensic analyst identify the accelerant used in an arson case using gas chromatography?

<p>By comparing gas chromatographic peaks from fire-scene debris to known flammable liquids. (B)</p> Signup and view all the answers

What is the purpose of using the ion mobility spectrometer mentioned in the text?

<p>Identifying explosive residues in materials collected for laboratory examination (B)</p> Signup and view all the answers

Why is it essential to collect and preserve loose soil and debris from the interior of a crater at the origin of an explosion?

<p>To analyze the debris by gas chromatography/mass spectrometry (C)</p> Signup and view all the answers

What is the purpose of rinsing recovered debris with organic solvents in forensic analysis?

<p>To identify accelerants used in the explosion (A)</p> Signup and view all the answers

Why is it important to use sealed air-tight containers for materials collected for laboratory examination?

<p>To prevent contamination of nearby containers by diffusing explosives (B)</p> Signup and view all the answers

What type of testing procedure is NOT mentioned as part of the analysis conducted on recovered debris?

<p>Vapor concentration technique (B)</p> Signup and view all the answers

Why are confirmatory identification tests performed on unexploded materials?

<p>To confirm the presence of explosives in the unexploded materials (D)</p> Signup and view all the answers

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