COPY: Extraction Techniques in Chemistry

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Questions and Answers

What is the purpose of the separatory funnel?

  • To measure the volume of a liquid
  • To separate liquids based on their densities (correct)
  • To heat a mixture of liquids
  • To mix liquids together

What happens when you shake the separatory funnel and allow the mixture to settle?

  • The mixture becomes homogeneous
  • The mixture becomes more viscous
  • The mixture separates into two distinct layers (correct)
  • The mixture evaporates quickly

What is the difference between the organic phase and the aqueous phase?

  • The organic phase is more dense, while the aqueous phase is less dense
  • The organic phase is acidic, while the aqueous phase is basic
  • The organic phase contains neutral compounds, while the aqueous phase contains water and ions (correct)
  • The organic phase contains water and ions, while the aqueous phase contains neutral compounds

Why do liquids separate into two distinct layers in the separatory funnel?

<p>Because they have different densities (B)</p> Signup and view all the answers

What is the function of the stopcock in the separatory funnel?

<p>To prevent liquid from flowing freely from the separatory funnel to the flask (C)</p> Signup and view all the answers

What is the first step in performing an extraction?

<p>Open the stopcock (C)</p> Signup and view all the answers

What is the purpose of extraction in the perfume industry?

<p>To isolate specific chemical compounds (D)</p> Signup and view all the answers

What is the name of the glassware used in extraction?

<p>Separatory funnel (A)</p> Signup and view all the answers

What is the purpose of adding hydrochloric acid to the mixture of hexane and propanamine?

<p>To protonate the amino group (C)</p> Signup and view all the answers

Why is sodium bicarbonate used in the extraction of acetic acid and phenol from hexane?

<p>Because it is a mild base that can deprotonate acetic acid but not phenol (B)</p> Signup and view all the answers

What happens to the phenol when sodium hydroxide is added to a mixture of hexane, phenol, and acetic acid?

<p>It becomes deprotonated and moves to the aqueous layer (D)</p> Signup and view all the answers

What is the purpose of separating the layers in an extraction process?

<p>To separate the compounds based on their properties (B)</p> Signup and view all the answers

What happens to the propanamine when hydrochloric acid is added to a mixture of hexane and propanamine?

<p>It becomes protonated and moves to the aqueous layer (B)</p> Signup and view all the answers

What is the advantage of using a multi-step extraction process?

<p>It allows for the recovery of products from waste containers (A)</p> Signup and view all the answers

Why is phenol weakly acidic?

<p>Because it has a weak hydroxyl group (A)</p> Signup and view all the answers

What is the purpose of adding a base to a mixture of hexane and phenol?

<p>To deprotonate the phenol (D)</p> Signup and view all the answers

What happens to the acetic acid when sodium bicarbonate is added to a mixture of hexane, acetic acid, and phenol?

<p>It becomes deprotonated and moves to the aqueous layer (D)</p> Signup and view all the answers

Why is it important to save each layer in an extraction process?

<p>Because some layers may contain valuable products (A)</p> Signup and view all the answers

Flashcards

Separatory Funnel Purpose?

Separates liquids based on density.

Shaking & Settling?

The mixture separates into distinct layers based on density.

Organic vs. Aqueous?

Organic phase: neutral compounds; aqueous phase: water and ions.

Stopcock Function?

To prevent free flow from the separatory funnel to the flask.

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First Extraction Step?

Open the stopcock.

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Extraction Purpose?

To isolate specific target chemical compounds.

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Extraction Glassware?

Separatory funnel.

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HCl Purpose?

Protonates the amino group, making it charged and water-soluble.

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Why Sodium Bicarbonate?

Mild base that deprotonates acetic acid, making it water-soluble, but does not deprotonate phenol.

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NaOH Effect on Phenol?

Phenol becomes deprotonated and moves to the aqueous layer.

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Layer Separation Purpose?

To separate compounds based on their properties (e.g., acidity, polarity).

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HCl Effect on Propanamine?

Propanamine becomes protonated and moves to the aqueous layer.

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Multi-Step Advantage?

It allows for the recovery of products from waste containers and ensures maximum yield.

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Why is Phenol Weakly Acidic?

It has a relatively stable conjugate base due to resonance delocalization.

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Base Addition Purpose?

To deprotonate the phenol, making it anionic and water-soluble.

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Bicarbonate Effect on Acetic Acid?

Acetic acid becomes deprotonated and moves to the aqueous layer.

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Save Each Layer?

Some layers may contain valuable products, ensuring nothing is wasted.

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