Chemistry Laboratory Apparatus Quiz

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Questions and Answers

In the chemistry laboratory, specific apparatus are needed to measure time, temperature, mass, and ______.

volume

The SI unit for time is the ______.

second

The temperature of a substance is measured using a ______.

thermometer

The SI unit for temperature is the ______.

<p>kelvin</p> Signup and view all the answers

Electronic balances have an accuracy of about ±______ g.

<p>0.01</p> Signup and view all the answers

Smaller volumes are measured in cubic decimetres (dm³) or cubic ______.

<p>centimetres</p> Signup and view all the answers

Longer intervals of time are measured in minutes (min) or ______.

<p>hours</p> Signup and view all the answers

1.25 liters is the same as ______ cm³.

<p>1250</p> Signup and view all the answers

A ______ can be used to measure the volume of a gas liberated during a chemical reaction.

<p>gas jar</p> Signup and view all the answers

The process of separating a soluble solid from an insoluble solid using a suitable solvent is known as ______.

<p>dissolution</p> Signup and view all the answers

To separate dry ice from common salt, we use the method of ______.

<p>sublimation</p> Signup and view all the answers

The insoluble solid remains in the filter funnel as residue during ______.

<p>filtration</p> Signup and view all the answers

A mixture of seawater can produce sea salt through the process of ______.

<p>evaporation</p> Signup and view all the answers

Measuring the melting point of a pure solid is an example of a ______ experiment.

<p>physical</p> Signup and view all the answers

The method of collecting gases lifted from a chemical reaction can include ______ delivery.

<p>downward</p> Signup and view all the answers

The liquid with the lowest boiling point is distilled ______.

<p>first</p> Signup and view all the answers

Fractional distillation is used to separate ______ into various useful fractions.

<p>petroleum</p> Signup and view all the answers

The boiling point of ______ gas is -152°C.

<p>Krypton</p> Signup and view all the answers

______ gas will distil out first because it has the lowest boiling point.

<p>Neon</p> Signup and view all the answers

Ethanol vaporises more ______, producing more ethanol vapour in the vapour phase.

<p>easily</p> Signup and view all the answers

Chromatography is used to separate two or more ______ in a mixture.

<p>substances</p> Signup and view all the answers

A ______ funnel is used to separate two immiscible liquids.

<p>separating</p> Signup and view all the answers

In a separating funnel, the denser liquid ______ to the bottom.

<p>sinks</p> Signup and view all the answers

More soluble substances move at a ______ rate in chromatography.

<p>faster</p> Signup and view all the answers

Copper(II) oxide is ______ in water.

<p>insoluble</p> Signup and view all the answers

A pure substance will produce ______ spot on the chromatogram.

<p>one</p> Signup and view all the answers

The more volatile liquid is the first to reach the top of the ______ column.

<p>fractionating</p> Signup and view all the answers

An impure substance will produce more than ______ spot on the chromatogram.

<p>one</p> Signup and view all the answers

The procedure for chromatography involves drawing a line with a ______ on filter paper.

<p>pencil</p> Signup and view all the answers

When all the ethanol has distilled over, the temperature will ______ again.

<p>rise</p> Signup and view all the answers

The first step in the chromatography process is to cut a ______-cm strip of filter paper.

<p>20</p> Signup and view all the answers

A mixture of amino acids can be separated by using ______ chromatography.

<p>paper</p> Signup and view all the answers

Amino acids are ______ substances.

<p>colourless</p> Signup and view all the answers

A locating agent called ______ is sprayed to help visualize the amino acids on the chromatogram.

<p>ninhydrin</p> Signup and view all the answers

The retention factor, or ______, is defined as the ratio of the distance moved by a component to the distance moved by the solvent front.

<p>R</p> Signup and view all the answers

To identify the amino acids in the mixture, calculated R values must be compared to those in a ______.

<p>database</p> Signup and view all the answers

One of the uses of paper chromatography is to detect ______ of products.

<p>purity</p> Signup and view all the answers

The start line on the chromatography paper should be drawn with a ______ rather than a ballpoint pen.

<p>pencil</p> Signup and view all the answers

If the solvent overshoots the top of the paper, accurate determination of the distance travelled by the ______ cannot be assessed.

<p>solvent</p> Signup and view all the answers

Pure ______ is used to make silicon chips for making microprocessors.

<p>silicon</p> Signup and view all the answers

Pure ______ is needed to make copper wires used in electrical wiring.

<p>copper</p> Signup and view all the answers

The melting point of pure tin is ______ °C.

<p>232</p> Signup and view all the answers

The presence of an impure substance will ______ the melting point of a pure substance.

<p>lower</p> Signup and view all the answers

The mixture of tin and lead with the lowest melting point contains ______% tin and ______% lead.

<p>64, 36</p> Signup and view all the answers

Methods of separation and purification include techniques such as filtration, ______, and distillation.

<p>crystallisation</p> Signup and view all the answers

Paper chromatography can be used to compare 'known' samples and deduce their ______.

<p>purity</p> Signup and view all the answers

Flashcards

Time Interval

The time interval between two events.

Second (s)

The standard unit of time measurement in the International System of Units (SI).

Stopwatch

An instrument used to measure the interval of time.

Temperature

The degree of hotness or coldness of a substance. It is measured using a thermometer.

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Kelvin (K)

The standard unit of temperature measurement in the International System of Units (SI).

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Celsius (°C)

A scale for measuring temperature where the freezing point of water is 0°C and the boiling point is 100°C.

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Mass

The amount of matter in an object. Measured using a balance.

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Kilogram (kg)

The standard unit of mass measurement in the International System of Units (SI).

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Dissolution

The process of separating a mixture of a soluble solid and an insoluble solid by dissolving the soluble solid in a suitable solvent.

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Sublimation

A technique used to separate a sublimable solid from a non-sublimable solid by heating the mixture. The sublimable solid changes directly from solid to gas, leaving the non-sublimable solid behind.

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Filtration

A method used to separate an insoluble solid from a liquid by passing the mixture through a filter paper. The solid residue remains on the filter paper, while the liquid filtrate passes through.

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Evaporation

A technique used to separate a dissolved solid from its solvent by heating the solution. The solvent evaporates, leaving the solid behind.

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Distillation

The process of separating a mixture by heating it, where the component with the lower boiling point vaporizes first and can be collected separately. This method is mainly used for mixtures of liquids.

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Fractional Distillation

A technique used to separate a mixture of two liquids with different boiling points by heating the mixture and collecting the vapor of the component with the lower boiling point.

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Separating Funnel

A method used to separate a mixture of two solids with different densities by using a separating funnel. The denser solid settles at the bottom, while the lighter solid stays at the top.

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Magnetic Separation

A technique used to separate a mixture of two solids with different magnetic properties by using a magnet. The magnetic solid is attracted to the magnet, while the non-magnetic solid remains unaffected.

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Chromatography

The process of separating a mixture into its individual components based on their different solubilities.

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Solubility and Chromatography

Substances that dissolve more easily travel faster in the chromatography process.

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Paper Chromatography

A chromatography method using paper strips to separate and identify substances.

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Pure Substance Chromatogram

A single substance will produce only one spot on a developed chromatogram.

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Impure Substance Chromatogram

A mixture will result in multiple spots on a developed chromatogram, with each spot representing a component of the mixture.

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Boiling Point and Liquefaction

A substance with a higher boiling point will liquefy first when a mixture of gases is cooled.

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Crystallization and Filtration

The process of separating solid crystals from a solution by filtering the solution through a filter paper to collect the crystals.

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Volatility

The ability of a substance to change from a liquid to a gas at a specific temperature. A more volatile substance will turn into a gas more easily.

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Fractionating Column

A tall, vertical column filled with glass beads or other packing material that helps separate liquids with different boiling points. The column provides a surface for repeated condensation and vaporization, increasing the purity of the collected liquids.

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Immiscible Liquids

Liquids that do not mix together, forming separate layers when combined. An example is oil and water.

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Soluble Solid

A solid that dissolves in a solvent, typically water.

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Insoluble Solid

A solid that does not dissolve in a solvent, such as water.

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Locating Agent (Ninhydrin)

A colorless chemical used to reveal the presence of amino acids on a chromatogram by reacting with them to form colored compounds.

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Retention Factor (Rf)

The ratio of the distance traveled by the center of a spot to the distance traveled by the solvent front. It helps identify components in a mixture.

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Start Line

The point where a sample is initially applied to the chromatography paper.

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Solvent Front

The highest point reached by the solvent on the chromatography paper. It helps determine the Rf value.

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Distance Moved by Component

The distance traveled by a component from the start line to its final position on the chromatogram.

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Distance Moved by Solvent

The distance traveled by the solvent front from the start line to its highest point on the chromatogram.

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Paper Chromatography for Amino Acid Separation

A technique used to analyze a mixture's components, particularly suitable for identifying colorless substances, like amino acids.

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Using a suitable solvent

A method used to separate mixtures based on the different solubilities of the components in a specific solvent. The soluble component dissolves in the solvent, while the insoluble component remains as a solid residue.

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Crystallisation

A technique used to obtain solid crystals from a saturated solution. The solution is heated to evaporate some of the solvent, making it more concentrated. As the solution cools, the solubility of the solute decreases, causing the excess solute to crystallize out.

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Study Notes

Experimental Design - Measurement

  • Specific laboratory equipment is needed for measuring time, temperature, mass, and volume
  • The International System of Units (SI units) is used for recording measurements
  • Time intervals are measured using stopwatches (analogue or digital)
    • The SI unit for time is the second (s)
    • Longer time intervals are measured in minutes (min) or hours (h)
    • Analogue stopwatches measure with an accuracy of ±0.1 s
    • Digital stopwatches measure with an accuracy of ±0.01 s
  • Temperature is measured using thermometers (analogue or digital)

Experimental Design - Temperature

  • The temperature of a substance is measured using a thermometer
  • Analogue and digital thermometers are both used
  • The SI unit for temperature is the kelvin (K)
  • Another common unit for temperature is the degree Celsius (°C)
  • The Kelvin scale starts at absolute zero (0 K), never negative
  • The Celsius scale is based on 0 °C for the freezing point of water and 100 °C for boiling point of water
  • To convert Celsius to Kelvin: K = °C + 273

Experimental Design - Mass

  • Mass is measured using electronic balances, chemical balances, or beam balances
  • The SI unit for mass is the kilogram (kg)
  • Smaller masses are measured in grams (g) or milligrams (mg), while larger masses are measured in tonnes (t)
  • Electronic balances typically have an accuracy of ±0.01 g

Experimental Design - Volume

  • The SI unit for volume is the cubic meter (m³)
  • Smaller volumes are measured in cubic decimeters (dm³) or cubic centimeters (cm³)
  • Measuring equipment includes burettes, measuring cylinders, pipettes, syringes, and volumetric flasks
  • The choice of apparatus depends on the volume to be measured and the accuracy required
  • A measuring cylinder is used to measure approximate volumes to the nearest 0.5 cm³
  • A gas syringe is used to measure gas volumes (up to 100cm³)
  • A burette is used to deliver accurate volumes (0-50 cm³ to ±0.05 cm³)
  • A pipette is used to deliver fixed volumes (usually 25 cm³)
  • A volumetric flask is used for accurate volume measurements

Experimental Design - Methods for Collecting Gases

  • Methods for collecting gases during chemical reactions depend on the gas's properties
    • By displacement of water (for insoluble gases e.g., hydrogen, nitrogen, oxygen, carbon dioxide)
    • By downward delivery (for gases denser than air, e.g., carbon dioxide, sulfur dioxide, hydrogen chloride)
    • By upward delivery (for gases less dense than air, e.g., ammonia, hydrogen)

Experimental Design - Drying Gases

  • The choice of drying agent depends on the gas properties
    • Neutral gases use sulfuric acid or fused calcium chloride
    • Acidic gases use sulfuric acid or fused calcium chloride
    • Alkaline gases use quicklime (calcium oxide)

Experimental Design - Titration

  • Titration is used to determine the concentration of a solution (often an acid-base reaction)
  • Equipment includes a burette (50 cm³), burette stand, conical flask, pipette

Experimental Design - Measuring Rates of Reactions

  • Measuring the change in volume of a liberated gas over time or measuring the change in mass of a reactant or product over time
  • Equipment includes graduated gas syringes, electronic balances, digital stopwatches

Experimental Design - Melting & Boiling Points

  • Measuring melting and boiling points to determine the identity of substances. Water cannot be used to heat substances with melting points above 100°C as paraffin oil is typically used instead
  • Pure substances have sharp melting and boiling points, while impure substances melt and boil over a range of temperatures. Impurities lower the melting point of substances and elevate the boiling points

Experimental Design - Chromatography

  • Chromatography is used to identify substances, determine purity, and separate mixtures
  • Different substances travel at different speeds due to varying solubilities in the solvent.
  • Paper chromatography is used in the lab with small quantity substances and mixtures with many substances
  • A pure substance produces one spot, the impure substance produces more than one spot.
  • Paper chromatography is used to separate and identify components in substances like ink and mixtures of amino acids
  • The retention factor (Rf) helps identify the components in the solution

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