Chemistry Gas Collection Methods
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Questions and Answers

Which of the following gases can be collected over water?

  • Hydrogen chloride
  • Oxygen (correct)
  • Sulfur dioxide
  • Ammonia
  • What is the appropriate method for collecting a gas that is soluble in water and denser than air?

  • Downward displacement of water
  • Downward delivery of gas (correct)
  • Upward delivery of gas
  • None of the above
  • Which of the following gases can be collected by downward displacement of water?

  • Chlorine
  • Carbon dioxide (correct)
  • Ammonia
  • Hydrogen chloride
  • Which method is suitable for collecting a gas that is less dense than air and insoluble in water?

    <p>Upward delivery (B)</p> Signup and view all the answers

    Which of the following is NOT a suitable drying agent for gases?

    <p>Sodium chloride (C)</p> Signup and view all the answers

    What is the most suitable method for collecting chlorine?

    <p>Downward delivery (A)</p> Signup and view all the answers

    What is the purpose of using fused calcium chloride to dry gases?

    <p>To remove moisture from the gas (B)</p> Signup and view all the answers

    A student needs to measure 25.0 cm³ of a liquid accurately. Which of the following pieces of equipment would be most suitable?

    <p>Pipette (A)</p> Signup and view all the answers

    A student is preparing to dissolve 4.08 g of solid sucrose in 43.00 cm³ of distilled water. Which of the following pieces of equipment would NOT be needed for this procedure?

    <p>Bunsen burner (C)</p> Signup and view all the answers

    Which of the following statements is TRUE for paper chromatography?

    <p>The stationary phase is the paper and the mobile phase is the solvent. (B)</p> Signup and view all the answers

    What is the volume of a gas collected in a gas syringe when it is measured to be at 50.0 mL?

    <p>50 cm³ (C)</p> Signup and view all the answers

    What is the Rf value used for in paper chromatography?

    <p>To identify the components of a mixture. (B)</p> Signup and view all the answers

    What is the advantage of using a locating agent in paper chromatography?

    <p>To make the colourless components visible. (C)</p> Signup and view all the answers

    What is the correct unit for measuring volume?

    <p>m³ (D)</p> Signup and view all the answers

    Which of the following is NOT an advantage of using paper chromatography?

    <p>It can be used to separate large quantities of components. (C)</p> Signup and view all the answers

    A student wants to accurately measure the volume of a liquid to the nearest 0.05 cm³. Which piece of apparatus should they use?

    <p>Burette (D)</p> Signup and view all the answers

    In the chromatogram, which solution(s) contain(s) only one dye?

    <p>Solution A (A)</p> Signup and view all the answers

    Which of the following describes the Rf value of a substance in chromatography?

    <p>The distance the substance travels relative to the distance the solvent travels (D)</p> Signup and view all the answers

    Why is it important that the start line in a chromatography experiment is not drawn in ink?

    <p>Ink will dissolve in the solvent and interfere with the separation process (C)</p> Signup and view all the answers

    In chromatography, why should the mixture samples on the start line be as small as possible?

    <p>To prevent the spots from merging together (A)</p> Signup and view all the answers

    Which separation method is most suitable for separating a mixture of two liquids that are miscible?

    <p>Fractional distillation (A)</p> Signup and view all the answers

    Which of the following is NOT a suitable method for separating a solid from a solution containing a soluble solid?

    <p>Filtration (D)</p> Signup and view all the answers

    Which separation technique is used to separate a mixture of two solids, one of which sublimes on heating?

    <p>Sublimation (B)</p> Signup and view all the answers

    Which of the following is a suitable method for separating a mixture of immiscible liquids?

    <p>Using a separating funnel (B)</p> Signup and view all the answers

    Which separation technique would be most suitable for separating a mixture of salt and sand?

    <p>Filtration (A)</p> Signup and view all the answers

    A mixture of iron filings and sulfur can be separated by:

    <p>Magnetic separation (B)</p> Signup and view all the answers

    Which of the following techniques would be most appropriate to separate a mixture of ethanol and water?

    <p>Distillation (C)</p> Signup and view all the answers

    Which of the following is a suitable locating agent in chromatography for colorless compounds?

    <p>All of the above (D)</p> Signup and view all the answers

    What does the Rf value in chromatography represent?

    <p>The ratio of the distance traveled by the substance to the distance traveled by the solvent (B)</p> Signup and view all the answers

    Two compounds have the following Rf values: Compound A - 0.45, Compound B - 0.78. If you ran a chromatography experiment and observed a spot with an Rf value of 0.75, which compound is it most likely to be?

    <p>Compound B (A)</p> Signup and view all the answers

    A mixture of sand, salt, and iron filings needs to be separated. What is the correct sequence of separation techniques to be used?

    <p>Magnetic separation, Filtration, Evaporation (C)</p> Signup and view all the answers

    What is a key requirement for successful distillation in separating a mixture?

    <p>Applying heat to the mixture until it boils. (B)</p> Signup and view all the answers

    When might fractional distillation be preferred over simple distillation?

    <p>When separating a mixture of two liquids with very similar boiling points. (D)</p> Signup and view all the answers

    What is the primary principle underlying the separation technique of chromatography?

    <p>Differences in the solubility of the components in the mobile phase. (D)</p> Signup and view all the answers

    What distinguishes sublimation from other separation techniques?

    <p>It requires the direct transition of a solid to a gas without passing through the liquid state. (C)</p> Signup and view all the answers

    What is the purpose of the starting line drawn in pencil in paper chromatography?

    <p>To mark the starting position of the mixture before the solvent is added. (A)</p> Signup and view all the answers

    Why is it important to heat the mixture until saturation during crystallisation?

    <p>To dissolve all the solute in the solvent. (A)</p> Signup and view all the answers

    What is the role of the separating funnel in separating immiscible liquids?

    <p>It allows the heavier liquid to be drained out first. (C)</p> Signup and view all the answers

    In filtration, what is the primary factor responsible for separating solids from liquids?

    <p>Differences in the solubility of the solid in the solvent used. (D)</p> Signup and view all the answers

    What would be the expected observation if an impure solid is heated to its melting point?

    <p>The solid will melt over a range of temperatures below the melting point of the pure solid. (D)</p> Signup and view all the answers

    In the process of distillation, why is the bulb of the thermometer placed at the outlet to the condenser?

    <p>To measure the temperature of the vapor being condensed. (D)</p> Signup and view all the answers

    Which of the following is a valid method for determining the purity of a substance?

    <p>Determining its boiling point (C)</p> Signup and view all the answers

    In chromatography, what does the presence of multiple faint spots on a chromatogram indicate?

    <p>The substance is a mixture of two or more components. (B)</p> Signup and view all the answers

    Why is ensuring the purity of substances important in the pharmaceutical industry?

    <p>To ensure the medicine has its original properties and avoids unwanted side effects. (A)</p> Signup and view all the answers

    During the process of obtaining sugar crystals from a sugar solution, how does the rate of cooling affect the size of the crystals formed?

    <p>Slower cooling leads to larger crystals. (A)</p> Signup and view all the answers

    Why is it important to add anti-bumping granules to the distillation flask?

    <p>To prevent the liquid from bumping and potentially breaking the flask. (B)</p> Signup and view all the answers

    What happens if a solution of copper (II) sulfate is heated till dryness?

    <p>Copper (II) oxide will be formed. (D)</p> Signup and view all the answers

    Flashcards

    Paper Chromatography

    A technique for separating mixtures based on the different rates at which components move across a medium.

    Distillation

    A separation technique that uses boiling and condensation to separate liquids based on different boiling points.

    Fractional Distillation

    A process that separates a mixture of liquids into its components using a fractionating column to enhance separation.

    Crystallization

    A process where a solid forms in a pure state from a solution as it cools or evaporates.

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    Sublimation

    A method of separation where a solid turns directly into gas without passing through a liquid state.

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    Separating Funnel

    A laboratory apparatus used for separating immiscible liquids based on their ability to not mix.

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    Filtration

    A technique that separates solids from liquids based on particle size or solubility differences in a solvent.

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    Chromatography Requirements

    In chromatography, a starting line needs to be drawn in pencil and not ink to prevent interference in results.

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    Separation Techniques

    Methods used to separate components in mixtures based on physical properties.

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    Liquid-Liquid Mixture

    A mixture where two liquids can be miscible (mix completely) or immiscible (not mix).

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    Evaporation

    The process of turning liquid into vapor, leaving solids behind.

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    Rf Value

    The ratio of the distance traveled by a substance to the distance traveled by the solvent in chromatography.

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    Locating Agents

    Substances used in chromatography to visualize colorless compounds.

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    Melting Point and Boiling Point

    The temperature at which a solid melts or a liquid boils, key for identifying substances.

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    Fused Calcium Chloride

    A drying agent that cannot dry ammonia due to forming ammine complexes.

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    Methods of Collecting Gases

    Techniques used to gather gases based on their solubility and density variations.

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    Hydrogen Collection

    Hydrogen is collected using an upward displacement of air due to being less dense than air.

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    Oxygen Collection

    Oxygen is collected using downward displacement of water as it is slightly denser than air.

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    Carbon Dioxide Collection

    Carbon dioxide is collected using downward displacement of water, as it is denser than air.

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    Principles of Chromatography

    Different components of a mixture travel at different speeds due to varying solubility in the solvent.

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    Using Locating Agents

    Locating agents reveal colorless spots on chromatograms by creating colored reactions.

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    Cubic metre (m³)

    The standard unit for measuring volume in the metric system.

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    Cubic centimetre (cm³)

    A smaller unit of volume measurement, often used for liquids.

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    Burette

    An instrument used to measure variable volumes of liquid accurately.

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    Gas syringe

    Device used to measure the volume of gases.

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    Downward displacement of water

    Method for collecting gases that are insoluble in water.

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    Upward delivery of gas

    Method for collecting gases that are less dense than air.

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    Drying agent

    Substances used to remove moisture from gases.

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    Concentrated sulfuric acid

    A strong drying agent used to remove moisture from gases.

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    Simple Distillation

    A process to separate a liquid from a solution by heating and cooling, collecting the vapor.

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    Separating Funnel Use

    A method for separating immiscible liquids, taking advantage of their differing densities.

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    Sugar Crystal Formation

    Method to obtain sugar crystals from a sugar solution by cooling and evaporation.

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    Temperature and Solubility

    Higher temperatures increase the solubility of sugar in water.

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    Cooling Rate and Crystal Size

    Faster cooling rates produce smaller crystals, while slower cooling creates larger ones.

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    Heating Sugars to Dryness

    Heating sugar or copper (II) sulfate solutions to dryness caramelizes or forms solid.

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    Thermometer Bulb Placement

    The thermometer bulb is placed at the condenser outlet to measure vapor temperature.

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    Cooling Water Direction in Distillation

    Cooling water enters the condenser at the bottom (B) to ensure effective cooling.

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    Antidumping Granules Purpose

    Antidumping granules prevent bumping during boiling in distillation.

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    Chromatography for Purity

    A technique showing purity through distinct spots: one for pure, multiple for impure.

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    Study Notes

    Experimental Chemistry Study Notes

    • Learning Outcomes (SIO 1.1a): Candidates should be able to identify appropriate apparatus for measuring time, temperature, mass, volume (including burettes, pipettes, measuring cylinders, and gas syringes).
    • Learning Outcomes (SIO 1.1b): Candidates should be able to suggest suitable apparatus and drying agents for various simple experiments, including drying agents (calcium oxide, concentrated sulfuric acid, and fused calcium chloride) and gas collection methods based on solubility and density.
    • Success Criteria (Unfamiliar): Specific criteria for each learning outcome detail the expected understanding and application of apparatus selection and gas collection based on various parameters.
    • Separation and Purification Methods (1.2a): Methods of separating and purifying mixtures include solvent use, filtration, crystallisation, evaporation, sublimation, distillation (including fractional distillation), separating funnels, and paper chromatography.
    • Paper Chromatography (1.2c): Identifying components in mixtures by comparing Rf values (distance travelled by a compound relative to the solvent).
    • Techniques for Determining Purity (1.2e): Melting point and boiling point data from substances can determine purity and identify the substance.
    • Importance of Purity (1.2f): Purity in different applications, such as food, drugs, and industry, is crucial for effectiveness and safety.
    • Measuring Physical Quantities (Key Concept A): The SI units for measuring mass, time, temperature, and volume, and the accuracy associated with common measuring tools (balances, stopwatches, thermometers, and measuring cylinders) are covered.
    • Methods of Collecting Gases (Key Concept B): Different methods, like downward displacement of water (insoluble or slightly soluble gases), downward delivery (soluble gases denser than air), and upward delivery (soluble gases less dense than air), are described based on the gas's solubility and density.
    • Drying Gases (Key Concept B): Methods for drying gases, such as using concentrated sulfuric acid or quicklime (calcium oxide), and considerations for using fused calcium chloride (limitations include ammonia, which forms a complex), are elaborated.
    • Paper Chromatography (Key Concept A): Applications and principles of paper chromatography for separating components in mixtures, identifying components, and assessing purity are discussed. Key factors include the solvent, travel speeds of different components, and calculating Rf values.
    • Criteria for Purity (Key Concept C): Two methods (melting point and boiling point) to determine the purity of a substance, along with their specific outcomes and observations for solids and liquids.
    • Impurities in a Substance (Key Concept C): Implications of impurities for different sectors such as industry (electronic and pharmaceutical) and everyday applications are highlighted.
    • Practical Applications of Separation Techniques: Explains how understanding and applying specific separation and purification techniques are vital in various sectors.

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    Description

    This quiz covers various methods of collecting gases, focusing on their solubility, density, and appropriate drying agents. Questions relate to practical laboratory techniques and equipment used in gas measurements and chromatography. Enhance your understanding of gas behavior and laboratory practices in chemistry.

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