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Questions and Answers
What occurs after the brief acceleration period in Type 1 settling?
What occurs after the brief acceleration period in Type 1 settling?
- The sedimentation rate remains constant immediately.
- The sediment begins to rise to the surface.
- The rate of sedimentation increases indefinitely.
- The interface moves downwards at a constant rate. (correct)
What happens when the interface approaches the layer of sediment in Type 1 settling?
What happens when the interface approaches the layer of sediment in Type 1 settling?
- The rate of fall decreases until the critical settling point is reached. (correct)
- The sediment continues to separate from the liquid.
- The suspension becomes fully homogenized.
- The liquid begins to separate from the solid particles.
Which factor does NOT affect the rate of sedimentation?
Which factor does NOT affect the rate of sedimentation?
- Temperature of the liquid. (correct)
- Shape of the vessel.
- Diameter of the containing vessel.
- Height of the suspension.
In Type 2 settling, what characterizes the sedimentation process?
In Type 2 settling, what characterizes the sedimentation process?
What is formed at the critical settling point in Type 1 settling?
What is formed at the critical settling point in Type 1 settling?
What is the primary characteristic of the separation process of a chemical mixture into pure components?
What is the primary characteristic of the separation process of a chemical mixture into pure components?
Which separation technique involves the transfer of species between vapor and liquid phases?
Which separation technique involves the transfer of species between vapor and liquid phases?
What type of separation technique adds another fluid phase to selectively absorb certain species from the feed?
What type of separation technique adds another fluid phase to selectively absorb certain species from the feed?
Which method uses a polymer membrane to exploit differences in species permeabilities?
Which method uses a polymer membrane to exploit differences in species permeabilities?
What is the common characteristic of the separation technique depicted as using a solid agent?
What is the common characteristic of the separation technique depicted as using a solid agent?
Which of the following is considered less common but of growing importance in separation techniques?
Which of the following is considered less common but of growing importance in separation techniques?
What does crystallization primarily exploit for the separation of species?
What does crystallization primarily exploit for the separation of species?
In liquid-liquid extraction, what characteristic must the added phase possess?
In liquid-liquid extraction, what characteristic must the added phase possess?
What is the primary purpose of thickening in the sedimentation process?
What is the primary purpose of thickening in the sedimentation process?
Which process involves the partial separation of suspended solid particles from a liquid by gravity?
Which process involves the partial separation of suspended solid particles from a liquid by gravity?
During sedimentation, what happens to the sedimentation rate once the critical settling point is reached?
During sedimentation, what happens to the sedimentation rate once the critical settling point is reached?
What characterizes the sedimentation process in a scenario with a wide range of particle sizes?
What characterizes the sedimentation process in a scenario with a wide range of particle sizes?
In the sedimentation process, what is typically seen at zone D?
In the sedimentation process, what is typically seen at zone D?
Which of the following external fields is particularly noted for its use in separating proteins?
Which of the following external fields is particularly noted for its use in separating proteins?
What is the end product of the clarification phase in sedimentation?
What is the end product of the clarification phase in sedimentation?
How is the sedimentation rate described before reaching the critical settling point?
How is the sedimentation rate described before reaching the critical settling point?
What is the terminal velocity of a particle in a fluid defined as?
What is the terminal velocity of a particle in a fluid defined as?
How does the presence of large particles affect a concentrated suspension?
How does the presence of large particles affect a concentrated suspension?
What happens to the apparent settling velocity in a concentrated suspension?
What happens to the apparent settling velocity in a concentrated suspension?
Which factor does NOT influence the calculation of the drag coefficient?
Which factor does NOT influence the calculation of the drag coefficient?
What is the form of the equation relating the drag force and the drag coefficient?
What is the form of the equation relating the drag force and the drag coefficient?
What physical principle primarily affects the behavior of particles in a fluid suspension?
What physical principle primarily affects the behavior of particles in a fluid suspension?
When does hindered settling occur?
When does hindered settling occur?
What aspect of fluid motion influences the velocity gradients near particles?
What aspect of fluid motion influences the velocity gradients near particles?
At which Reynolds number does Stokes' law apply?
At which Reynolds number does Stokes' law apply?
What is the drag coefficient for Reynolds numbers between 500 and 200,000?
What is the drag coefficient for Reynolds numbers between 500 and 200,000?
In which region is the settling velocity given by $u_s = \frac{0.153g d^3 (\rho_s - \rho_f)}{\rho_f \mu}$?
In which region is the settling velocity given by $u_s = \frac{0.153g d^3 (\rho_s - \rho_f)}{\rho_f \mu}$?
What is the empirical equation to determine settling for particle sizes using the highest Reynolds number?
What is the empirical equation to determine settling for particle sizes using the highest Reynolds number?
What is the drag force equation applicable for Reynolds numbers between 500 and 200,000?
What is the drag force equation applicable for Reynolds numbers between 500 and 200,000?
What defines the criterion for the empirical equation in determining settling velocity?
What defines the criterion for the empirical equation in determining settling velocity?
What does the constant K_c depend on?
What does the constant K_c depend on?
If a particle is in a low Reynolds number region, which equation best describes the settling velocity?
If a particle is in a low Reynolds number region, which equation best describes the settling velocity?
Flashcards
Sedimentation
Sedimentation
Separation of solid particles suspended in a liquid using gravity.
Thickening
Thickening
The process of increasing the concentration of suspended solids in a liquid by sedimentation.
Clarification
Clarification
The process of removing suspended solids from a liquid to produce a clear effluent.
Zone C
Zone C
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Critical Settling Point
Critical Settling Point
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Constant Composition Sedimentation
Constant Composition Sedimentation
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Variable Composition Sedimentation
Variable Composition Sedimentation
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Sedimentation Rate
Sedimentation Rate
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Separation
Separation
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Mixture Formation
Mixture Formation
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Separation by Phase Creation
Separation by Phase Creation
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Separation by Phase Addition
Separation by Phase Addition
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Separation by Barrier
Separation by Barrier
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Separation by Solid Agent
Separation by Solid Agent
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Distillation
Distillation
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Crystallization
Crystallization
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Type 1 Settling
Type 1 Settling
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Type 2 Settling
Type 2 Settling
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Settling Velocity
Settling Velocity
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Factors Affecting Sedimentation Rate
Factors Affecting Sedimentation Rate
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Hindered Settling
Hindered Settling
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Size Range Effect on Settling
Size Range Effect on Settling
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Fluid Displacement
Fluid Displacement
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Velocity Gradients
Velocity Gradients
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Terminal Velocity
Terminal Velocity
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Drag Force Equation
Drag Force Equation
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Drag Coefficient
Drag Coefficient
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Brownian Motion
Brownian Motion
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Reynolds number
Reynolds number
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Stokes' Law
Stokes' Law
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Kc (Settling Parameter)
Kc (Settling Parameter)
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Reynolds Region
Reynolds Region
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Stokes Region
Stokes Region
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Transition Region
Transition Region
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Empirical Settling Equation (Equation 6)
Empirical Settling Equation (Equation 6)
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Study Notes
Basic Separation Techniques
- Separation of chemical mixtures is not a spontaneous process, requiring energy input
- Multiphase mixtures are often separated into individual phases first
- Common separation techniques are diagrammed in Figure 1.1
- Separation by phase creation (Figure 1.1a)
- Separation by phase addition (Figure 1.1b)
- Separation by barrier (Figure 1.1c)
- Separation by solid agent (Figure 1.1d)
- Separation by force field or gradient (Figure 1.1e)
- The most common technique creates a second, immiscible phase (Figure 1.1a)
Sedimentation
-
Mechanical separation of one bulk phase from another
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Separates suspended solids from a liquid via gravity settling
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Operations include thickening and clarification
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Thickening increases solid concentration
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Clarification produces a clear effluent (liquid)
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Sedimentation occurs in one or two ways (Figure 2a)
- Clear liquid (A)
- Suspension (B)
- Gradual increase in concentration (C)
- Sediment layer (D)
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Sedimentation rate varies with particle size distribution (Figure 2b)
Settling Velocity
- Terminal velocity (ut) is the velocity at which a particle stops accelerating due to gravity
- Drag force and buoyant force balance gravity force
- Settling velocity affected by fluid height, vessel diameter, volumetric concentration, and shape (of the vessel)
Reynolds Number Region
- Stokes' law (Equation 3) applies at low Reynolds numbers (NRe < ~2)
- For intermediate Reynolds numbers (500 to 200,000), drag coefficient is relatively constant for spherical particles
- Newton's Law is applicable for higher Reynolds numbers
- Ranges of equations for different Reynolds numbers (Table 2)
Flocculation
- Enhances sedimentation by causing small particles to aggregate into larger, faster-settling flocs
- Coagulation and flocculation may occur sequentially or concurrently
- Flocculation is the agglomeration of flocs formed during coagulation
- Figure 3 shows the process of coagulation, flocculation, and subsequent sedimentation
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